methyl 4-(4-(3-(4-cyano-2-fluoro-3-(trifluoromethyl)phenyl)-5,5-dimethyl-4-oxo-2-thioxoimidazolidin-1-yl)phenyl)butanoate

Base Information

Chemical Name:methyl 4-(4-(3-(4-cyano-2-fluoro-3-(trifluoromethyl)phenyl)-5,5-dimethyl-4-oxo-2-thioxoimidazolidin-1-yl)phenyl)butanoate
CAS No.:1398044-97-7
Molecular Formula:C₂₄H₂₁F₄N₃O₃S
Molecular Weight:507.509
Hs Code.:

Synonyms:methyl 4-(4-(3-(4-cyano-2-fluoro-3-(trifluoromethyl)phenyl)-5,5-dimethyl-4-oxo-2-thioxoimidazolidin-1-yl)phenyl)butanoate

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Chemical Property of methyl 4-(4-(3-(4-cyano-2-fluoro-3-(trifluoromethyl)phenyl)-5,5-dimethyl-4-oxo-2-thioxoimidazolidin-1-yl)phenyl)butanoate

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Technology Process of methyl 4-(4-(3-(4-cyano-2-fluoro-3-(trifluoromethyl)phenyl)-5,5-dimethyl-4-oxo-2-thioxoimidazolidin-1-yl)phenyl)butanoate

There total 3 articles about methyl 4-(4-(3-(4-cyano-2-fluoro-3-(trifluoromethyl)phenyl)-5,5-dimethyl-4-oxo-2-thioxoimidazolidin-1-yl)phenyl)butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1311158-94-7
C₉H₂F₄N₂S

: 1398046-74-6
methyl 4-(4-((2-cyanopropan-2-yl)amino)phenyl)butanoate

: 1398044-97-7
methyl 4-(4-(3-(4-cyano-2-fluoro-3-(trifluoromethyl)phenyl)-5,5-dimethyl-4-oxo-2-thioxoimidazolidin-1-yl)phenyl)butanoate

Guidance literature:: C₉H₂F₄N₂S; methyl 4-(4-((2-cyanopropan-2-yl)amino)phenyl)butanoate; In N,N-dimethyl-formamide; at 20 ℃;

With hydrogenchloride; water; In methanol; N,N-dimethyl-formamide; for 2h; Reflux;

Reference yield:

: 15118-60-2
4-(4-aminophenyl)butyric Acid

: 1398044-97-7
methyl 4-(4-(3-(4-cyano-2-fluoro-3-(trifluoromethyl)phenyl)-5,5-dimethyl-4-oxo-2-thioxoimidazolidin-1-yl)phenyl)butanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: thionyl chloride / methanol / 16 h / 0 - 80 °C

2.1: iodine / 0.5 h / 50 °C

3.1: N,N-dimethyl-formamide / 20 °C

3.2: 2 h / Reflux

With thionyl chloride; iodine; In methanol; N,N-dimethyl-formamide;

Reference yield:

: 20637-09-6
methyl 4-(4-aminophenyl)butanoate

: 1398044-97-7
methyl 4-(4-(3-(4-cyano-2-fluoro-3-(trifluoromethyl)phenyl)-5,5-dimethyl-4-oxo-2-thioxoimidazolidin-1-yl)phenyl)butanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: iodine / 0.5 h / 50 °C

2.1: N,N-dimethyl-formamide / 20 °C

2.2: 2 h / Reflux

iodine; In N,N-dimethyl-formamide;