N-acetyl kynuramine methyl carbamate

Base Information

• Chemical Name: N-acetyl kynuramine methyl carbamate
• CAS No.: 1430088-58-6
• Molecular Formula: C₁₃H₁₆N₂O₄
• Molecular Weight: 264.281
• Mol file: 1430088-58-6.mol

Synonyms:N-acetyl kynuramine methyl carbamate

Chemical Property of N-acetyl kynuramine methyl carbamate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-acetyl kynuramine methyl carbamate

There total 2 articles about N-acetyl kynuramine methyl carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

methyl 2-(1-H-indol-3-yl)ethylcarbamate (58635-45-3) + acetic acid (64-19-7,77671-22-8) → N-acetyl kynuramine methyl carbamate (1430088-58-6) + kynuramine methyl carbamate (63637-61-6)

Guidance literature:

methyl 2-(1-H-indol-3-yl)ethylcarbamate; acetic acid; With ozone; Cooling with ice;

With hydrogenchloride; In water; at 40 ℃; for 1.5h;

DOI:10.3390/md11020274

Reference yield:

tryptamine (61-54-1) → N-acetyl kynuramine methyl carbamate (1430088-58-6) + kynuramine methyl carbamate (63637-61-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: sodium hydroxide / water; ethyl acetate / 0.5 h / 20 °C / Inert atmosphere

2.1: ozone / Cooling with ice

2.2: 1.5 h / 40 °C

With ozone; sodium hydroxide; In water; ethyl acetate;

DOI:10.3390/md11020274

upstream raw materials:

tryptamine

methyl 2-(1-H-indol-3-yl)ethylcarbamate

acetic acid