OP(C₆H₅)(C₆H₄P(C₆H₅)(N(CH(CH₃)2)2)O)2

Base Information

Chemical Name:OP(C₆H₅)(C₆H₄P(C₆H₅)(N(CH(CH₃)2)2)O)2
CAS No.:1314006-35-3
Molecular Formula:C₄₂H₅₁N₂O₃P₃
Molecular Weight:724.8
Hs Code.:

OP(C<sub>6</sub>H<sub>5</sub>)(C<sub>6</sub>H<sub>4</sub>P(C<sub>6</sub>H<sub>5</sub>)(N(CH(CH<sub>3</sub>)2)2)O)2

Synonyms:OP(C₆H₅)(C₆H₄P(C₆H₅)(N(CH(CH₃)2)2)O)2

Suppliers and Price of OP(C₆H₅)(C₆H₄P(C₆H₅)(N(CH(CH₃)2)2)O)2

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of OP(C₆H₅)(C₆H₄P(C₆H₅)(N(CH(CH₃)2)2)O)2

Chemical Property:

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Technology Process of OP(C₆H₅)(C₆H₄P(C₆H₅)(N(CH(CH₃)2)2)O)2

There total 1 articles about OP(C₆H₅)(C₆H₄P(C₆H₅)(N(CH(CH₃)2)2)O)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 824-72-6
P,P-dichlorophenylphosphine oxide

: 131173-04-1
N,N-Di-isopropyl-P,P-diphenylphosphinic amide

: 1314006-35-3
OP(C₆H₅)(C₆H₄P(C₆H₅)(N(CH(CH₃)2)2)O)2

Guidance literature:: N,N-Di-isopropyl-P,P-diphenylphosphinic amide; With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In hexane; toluene; at -90 ℃; for 1h; Inert atmosphere;

P,P-dichlorophenylphosphine oxide; In hexane; toluene; at -90 - 20 ℃; diastereoselective reaction; Inert atmosphere;
DOI:10.1039/c1dt10194c

Reference yield:

: yttrium(lll) nitrate hexahydrate

: 1314006-35-3
OP(C₆H₅)(C₆H₄P(C₆H₅)(N(CH(CH₃)2)2)O)2

: (Y(OP(C₆H₅)(C₆H₄P(C₆H₅)(N(CH(CH₃)2)2)O)2)(NO₃)3)

Guidance literature:: In acetonitrile; (N2) to suspn. ligand in MeCN Y(NO3)3*6H2O was added (2:1), stirred for 4 days; soln. was evapd. slowly, residue was recrystd. from MeCN layered with Et2O; elem. anal.;
DOI:10.1039/c1dt10194c

Reference yield:

: yttrium(lll) nitrate hexahydrate

: 1314006-35-3
OP(C₆H₅)(C₆H₄P(C₆H₅)(N(CH(CH₃)2)2)O)2

: (Y(OP(C₆H₅)(C₆H₄P(C₆H₅)(N(CH(CH₃)2)2)O)2)2(NO₃))⁽²⁺⁾*2NO₃^(1-)=(Y(OP(C₆H₅)(C₆H₄P(C₆H₅)(N(CH(CH₃)2)2)O)2)2(NO₃))(NO₃)2

Guidance literature:: In acetonitrile; (N2) to suspn. ligand in MeCN Y(NO3)3*6H2O was added (1:1), stirred for 15 min; soln. was evapd. slowly, residue was recrystd. from MeCN layered with Et2O; elem. anal.;
DOI:10.1039/c1dt10194c