Methyl-2-benzamido-2,5,6-tridesoxy-5,6-epithio-3-O-<(1R)-1-(4-nitrophenoxycarbonyl)ethyl>-β-D-glucofuranosid

Base Information

Chemical Name:Methyl-2-benzamido-2,5,6-tridesoxy-5,6-epithio-3-O-<(1R)-1-(4-nitrophenoxycarbonyl)ethyl>-β-D-glucofuranosid
CAS No.:106947-94-8
Molecular Formula:C₂₃H₂₄N₂O₈S
Molecular Weight:488.518
Hs Code.:

Synonyms:Methyl-2-benzamido-2,5,6-tridesoxy-5,6-epithio-3-O-<(1R)-1-(4-nitrophenoxycarbonyl)ethyl>-β-D-glucofuranosid

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Chemical Property of Methyl-2-benzamido-2,5,6-tridesoxy-5,6-epithio-3-O-<(1R)-1-(4-nitrophenoxycarbonyl)ethyl>-β-D-glucofuranosid

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Technology Process of Methyl-2-benzamido-2,5,6-tridesoxy-5,6-epithio-3-O-<(1R)-1-(4-nitrophenoxycarbonyl)ethyl>-β-D-glucofuranosid

There total 9 articles about Methyl-2-benzamido-2,5,6-tridesoxy-5,6-epithio-3-O-<(1R)-1-(4-nitrophenoxycarbonyl)ethyl>-β-D-glucofuranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 106948-01-0
Methyl-5,6-anhydro-2-benzamido-2-desoxy-3-O-<(1R)-1-(4-nitrophenoxycarbonyl)ethyl>-α-L-idofuranosid

: 106947-94-8
Methyl-2-benzamido-2,5,6-tridesoxy-5,6-epithio-3-O-<(1R)-1-(4-nitrophenoxycarbonyl)ethyl>-β-D-glucofuranosid

Guidance literature:: With triphenylphosphine sulfide; trifluoroacetic acid; In chloroform; at 40 ℃; for 12h;

Reference yield:

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 106947-94-8
Methyl-2-benzamido-2,5,6-tridesoxy-5,6-epithio-3-O-<(1R)-1-(4-nitrophenoxycarbonyl)ethyl>-β-D-glucofuranosid

Guidance literature:: Multi-step reaction with 2 steps

1: 45 percent / DCC / ethyl acetate / 1.) 0 deg C, 30 min, 2.) room temp., 5 h

2: 42 percent / (C₆H₅)3PS, CF₃COOH / CHCl₃ / 12 h / 40 °C

With dicyclohexyl-carbodiimide; triphenylphosphine sulfide; trifluoroacetic acid; In chloroform; ethyl acetate;

Reference yield:

: 106947-89-1
Methyl-2-benzamido-3-O-<(1R)-1-carboxyethyl>-2-desoxy-β-D-glucofuranosid

: 106947-94-8
Methyl-2-benzamido-2,5,6-tridesoxy-5,6-epithio-3-O-<(1R)-1-(4-nitrophenoxycarbonyl)ethyl>-β-D-glucofuranosid

Guidance literature:: Multi-step reaction with 6 steps

1: 58 percent / DCC, DMAP / tetrahydrofuran / 24 h / Ambient temperature

2: 58 percent / pyridine / 16 h / -10 °C

3: 54 percent / pyridine / 16 h / Ambient temperature

4: 93 percent / CH₃ONa / tetrahydrofuran / 0.5 h / 0 °C

5: 45 percent / DCC / ethyl acetate / 1.) 0 deg C, 30 min, 2.) room temp., 5 h

6: 42 percent / (C₆H₅)3PS, CF₃COOH / CHCl₃ / 12 h / 40 °C

With pyridine; dmap; sodium methylate; dicyclohexyl-carbodiimide; triphenylphosphine sulfide; trifluoroacetic acid; In tetrahydrofuran; chloroform; ethyl acetate;