(2S,4S,8S)-di-tert-butyl 5-oxo-4-benzyl-2,8-di-[N-(9-(9-phenylfluorenyl))amino]azelate

Base Information

Chemical Name:(2S,4S,8S)-di-tert-butyl 5-oxo-4-benzyl-2,8-di-[N-(9-(9-phenylfluorenyl))amino]azelate
CAS No.:213415-99-7
Molecular Formula:C₆₂H₆₂N₂O₅
Molecular Weight:915.185
Hs Code.:

Synonyms:(2S,4S,8S)-di-tert-butyl 5-oxo-4-benzyl-2,8-di-[N-(9-(9-phenylfluorenyl))amino]azelate

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Chemical Property of (2S,4S,8S)-di-tert-butyl 5-oxo-4-benzyl-2,8-di-[N-(9-(9-phenylfluorenyl))amino]azelate

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Technology Process of (2S,4S,8S)-di-tert-butyl 5-oxo-4-benzyl-2,8-di-[N-(9-(9-phenylfluorenyl))amino]azelate

There total 4 articles about (2S,4S,8S)-di-tert-butyl 5-oxo-4-benzyl-2,8-di-[N-(9-(9-phenylfluorenyl))amino]azelate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 100-39-0
benzyl bromide

: 159303-53-4
(2S,8S)-di-tert-butyl 5-oxo-2,8-di-[N-(9-(9-phenylfluorenyl))amino]azelate

: 213416-00-3
(2S,4R,8S)-di-tert-butyl 5-oxo-4-benzyl-2,8-di-[N-(9-(9-phenylfluorenyl))amino]azelate

: 213415-99-7
(2S,4S,8S)-di-tert-butyl 5-oxo-4-benzyl-2,8-di-[N-(9-(9-phenylfluorenyl))amino]azelate

: (2S,4R,6R,8S)-di-tert-butyl 5-oxo-4,6-dibenzyl-2,8-di-[N-(9-(9-phenylfluorenyl))amino]azelate

Guidance literature:: (2S,8S)-di-tert-butyl 5-oxo-2,8-di-[N-(9-(9-phenylfluorenyl))amino]azelate; With potassium hexamethylsilazane; In tetrahydrofuran; toluene; at -78 ℃; for 1h;

benzyl bromide; In tetrahydrofuran; toluene; at -78 - -10 ℃; for 3.25h;
DOI:10.1021/jo980596x

Reference yield: 31.0%

: 100-39-0
benzyl bromide

: 159303-53-4
(2S,8S)-di-tert-butyl 5-oxo-2,8-di-[N-(9-(9-phenylfluorenyl))amino]azelate

: 213416-00-3
(2S,4R,8S)-di-tert-butyl 5-oxo-4-benzyl-2,8-di-[N-(9-(9-phenylfluorenyl))amino]azelate

: 213415-99-7
(2S,4S,8S)-di-tert-butyl 5-oxo-4-benzyl-2,8-di-[N-(9-(9-phenylfluorenyl))amino]azelate

: (2S,4S,6R,8S)-di-tert-butyl 5-oxo-4,6-dibenzyl-2,8-di-[N-(9-(9-phenylfluorenyl))amino]azelate

: (2S,4R,6R,8S)-di-tert-butyl 5-oxo-4,6-dibenzyl-2,8-di-[N-(9-(9-phenylfluorenyl))amino]azelate

Guidance literature:: (2S,8S)-di-tert-butyl 5-oxo-2,8-di-[N-(9-(9-phenylfluorenyl))amino]azelate; With potassium hexamethylsilazane; In tetrahydrofuran; toluene; at -78 ℃; for 0.5h;

benzyl bromide; With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; In tetrahydrofuran; toluene; at -78 ℃;
DOI:10.1021/jo980596x

Reference yield: 14.0%

: 100-39-0
benzyl bromide

: 159303-53-4
(2S,8S)-di-tert-butyl 5-oxo-2,8-di-[N-(9-(9-phenylfluorenyl))amino]azelate

: 213416-00-3
(2S,4R,8S)-di-tert-butyl 5-oxo-4-benzyl-2,8-di-[N-(9-(9-phenylfluorenyl))amino]azelate

: 213415-99-7
(2S,4S,8S)-di-tert-butyl 5-oxo-4-benzyl-2,8-di-[N-(9-(9-phenylfluorenyl))amino]azelate

Guidance literature:: (2S,8S)-di-tert-butyl 5-oxo-2,8-di-[N-(9-(9-phenylfluorenyl))amino]azelate; With potassium hexamethylsilazane; In tetrahydrofuran; toluene; at -78 ℃; for 0.5h;

benzyl bromide; With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; In tetrahydrofuran; toluene; at -78 ℃;
DOI:10.1021/jo980596x