2-Methyl-5-(4-nitrobenzoyl)amino-2H-benzotriazole

Base Information

Chemical Name:2-Methyl-5-(4-nitrobenzoyl)amino-2H-benzotriazole
CAS No.:142312-67-2
Molecular Formula:C₁₄H₁₁N₅O₃
Molecular Weight:297.273
Hs Code.:
DSSTox Substance ID:DTXSID10872255
Nikkaji Number:J483.161F

Synonyms:142312-67-2;DTXSID10872255;N-(2-methylbenzotriazol-5-yl)-4-nitro-benzamide;2-Methyl-5-(4-nitrobenzoyl)amino-2H-benzotriazole;N-(2-Methyl-2H-benzotriazol-5-yl)-4-nitrobenzamide;Benzamide, N-(2-methyl-2H-1,2,3-benzotriazol-5-yl)-4-nitro-

Suppliers and Price of 2-Methyl-5-(4-nitrobenzoyl)amino-2H-benzotriazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Methyl-5-(4-nitrobenzoyl)amino-2H-benzotriazole

Chemical Property:

XLogP3:2.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:2
Exact Mass:297.08618923
Heavy Atom Count:22
Complexity:433

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CN1N=C2C=CC(=CC2=N1)NC(=O)C3=CC=C(C=C3)[N+](=O)[O-]

Technology Process of 2-Methyl-5-(4-nitrobenzoyl)amino-2H-benzotriazole

There total 3 articles about 2-Methyl-5-(4-nitrobenzoyl)amino-2H-benzotriazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 89852-83-5
2-methyl-2H-benzo[d][1,2,3]triazol-5-amine

: 122-04-3
4-nitro-benzoyl chloride

: 142312-67-2
N-(2-Methyl-2H-benzotriazol-5-yl)-4-nitro-benzamide

Guidance literature:: With pyridine; In benzene; for 4h; Heating;
DOI:10.1016/0223-5234(92)90105-A

Reference yield:

: 36793-96-1
2-methyl-5-nitro-2H-benzotriazole

: 142312-67-2
N-(2-Methyl-2H-benzotriazol-5-yl)-4-nitro-benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / 10percent Pd/activated C / methanol / Ambient temperature

2: 48 percent / pyridine / benzene / 4 h / Heating

With pyridine; hydrogen; palladium on activated charcoal; In methanol; benzene;
DOI:10.1016/0223-5234(92)90105-A

Reference yield:

: 2338-12-7
5-nitrobenzotriazole

: 142312-67-2
N-(2-Methyl-2H-benzotriazol-5-yl)-4-nitro-benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: 59 percent / EtONa / ethanol / 24 h / Heating

2: H₂ / 10percent Pd/activated C / methanol / Ambient temperature

3: 48 percent / pyridine / benzene / 4 h / Heating

With pyridine; hydrogen; sodium ethanolate; palladium on activated charcoal; In methanol; ethanol; benzene;
DOI:10.1016/0223-5234(92)90105-A