(2S)-N-(4-benzyloxy-5-methoxy-2-nitrobenzoyl)-2-(hydroxymethyl)-4-methylidenepyrrolidine

Base Information

Chemical Name:(2S)-N-(4-benzyloxy-5-methoxy-2-nitrobenzoyl)-2-(hydroxymethyl)-4-methylidenepyrrolidine
CAS No.:260418-16-4
Molecular Formula:C₂₁H₂₂N₂O₆
Molecular Weight:398.415
Hs Code.:

Synonyms:(2S)-N-(4-benzyloxy-5-methoxy-2-nitrobenzoyl)-2-(hydroxymethyl)-4-methylidenepyrrolidine

Suppliers and Price of (2S)-N-(4-benzyloxy-5-methoxy-2-nitrobenzoyl)-2-(hydroxymethyl)-4-methylidenepyrrolidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S)-N-(4-benzyloxy-5-methoxy-2-nitrobenzoyl)-2-(hydroxymethyl)-4-methylidenepyrrolidine

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Technology Process of (2S)-N-(4-benzyloxy-5-methoxy-2-nitrobenzoyl)-2-(hydroxymethyl)-4-methylidenepyrrolidine

There total 11 articles about (2S)-N-(4-benzyloxy-5-methoxy-2-nitrobenzoyl)-2-(hydroxymethyl)-4-methylidenepyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: (2S)-N-(4-benzyloxy-5-methoxy-2-nitrobenzoyl)-2-(tert-butyldimethylsilyloxymethyl)-4-methylidenepyrrolidine

: 260418-16-4
(2S)-N-(4-benzyloxy-5-methoxy-2-nitrobenzoyl)-2-(hydroxymethyl)-4-methylidenepyrrolidine

Guidance literature:: With acetic acid; In tetrahydrofuran; water; at 20 ℃; for 16h; Inert atmosphere;

Reference yield: 79.0%

: 926279-19-8
(S)-(4-methylenepyrrolidin-2-yl)methanol hydrochloride salt

: 60547-92-4
4-(benzyloxy)-5-methoxy-2-nitrobenzoic acid

: 260418-16-4
(2S)-N-(4-benzyloxy-5-methoxy-2-nitrobenzoyl)-2-(hydroxymethyl)-4-methylidenepyrrolidine

Guidance literature:: 4-(benzyloxy)-5-methoxy-2-nitrobenzoic acid; With oxalyl dichloride; In dichloromethane; N,N-dimethyl-formamide; at 20 ℃; for 2h;

(S)-(4-methylenepyrrolidin-2-yl)methanol hydrochloride salt; With triethylamine; acetyl chloride; In dichloromethane; at 0 - 20 ℃; for 8h; Inert atmosphere;