Technology Process of C49H42N2O6
There total 7 articles about C49H42N2O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride;
In
toluene;
for 2h;
Heating;
DOI:10.1021/ja046965q
- Guidance literature:
-
Multi-step reaction with 7 steps
1: K2CO3 / acetone / 16 h / Heating
2: LiAlH4 / tetrahydrofuran / 30 °C
3: PBr3; pyridine / CH2Cl2
4: K2CO3 / acetone / 16 h / Heating
5: pyridinium chlorochromate / CH2Cl2 / 1 h
6: 86 percent / ethanol; diethyl ether / 12 h / Heating
7: aq. NaOH; Et3BnNCl / toluene / 2 h / Heating
With
pyridine; sodium hydroxide; lithium aluminium tetrahydride; N-benzyl-N,N,N-triethylammonium chloride; phosphorus tribromide; potassium carbonate; pyridinium chlorochromate;
In
tetrahydrofuran; diethyl ether; ethanol; dichloromethane; acetone; toluene;
7: Bamford-Stevens reaction;
DOI:10.1021/ja046965q
- Guidance literature:
-
Multi-step reaction with 5 steps
1: PBr3; pyridine / CH2Cl2
2: K2CO3 / acetone / 16 h / Heating
3: pyridinium chlorochromate / CH2Cl2 / 1 h
4: 86 percent / ethanol; diethyl ether / 12 h / Heating
5: aq. NaOH; Et3BnNCl / toluene / 2 h / Heating
With
pyridine; sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; phosphorus tribromide; potassium carbonate; pyridinium chlorochromate;
In
diethyl ether; ethanol; dichloromethane; acetone; toluene;
5: Bamford-Stevens reaction;
DOI:10.1021/ja046965q