(2S,5S,6R)-6-(2,5-dimethoxyphenyl)-2,6-dimethoxy-1-hydroxy-5-methylhex-3-enyl-(E)-(1R)-acetylmandelic acid

Base Information

Chemical Name:(2S,5S,6R)-6-(2,5-dimethoxyphenyl)-2,6-dimethoxy-1-hydroxy-5-methylhex-3-enyl-(E)-(1R)-acetylmandelic acid
CAS No.:134333-59-8
Molecular Formula:C₂₇H₃₄O₈
Molecular Weight:486.562
Hs Code.:

Synonyms:(2S,5S,6R)-6-(2,5-dimethoxyphenyl)-2,6-dimethoxy-1-hydroxy-5-methylhex-3-enyl-(E)-(1R)-acetylmandelic acid

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Chemical Property of (2S,5S,6R)-6-(2,5-dimethoxyphenyl)-2,6-dimethoxy-1-hydroxy-5-methylhex-3-enyl-(E)-(1R)-acetylmandelic acid

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Technology Process of (2S,5S,6R)-6-(2,5-dimethoxyphenyl)-2,6-dimethoxy-1-hydroxy-5-methylhex-3-enyl-(E)-(1R)-acetylmandelic acid

There total 4 articles about (2S,5S,6R)-6-(2,5-dimethoxyphenyl)-2,6-dimethoxy-1-hydroxy-5-methylhex-3-enyl-(E)-(1R)-acetylmandelic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 74327-86-9
α,α,2,5-tetramethoxytoluene

: 134333-59-8
(2S,5S,6R)-6-(2,5-dimethoxyphenyl)-2,6-dimethoxy-1-hydroxy-5-methylhex-3-enyl-(E)-(1R)-acetylmandelic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / trimethylsilyl trifluoromethanesulfonate / CH₂Cl₂ / 6 h / -78 °C

2: LiAlH₄ / tetrahydrofuran / 0.25 h / 0 °C

3: DMAP, 1,3-dicyclohexylcarbodiimide / CH₂Cl₂ / 8 h / Ambient temperature

With dmap; lithium aluminium tetrahydride; trimethylsilyl trifluoromethanesulfonate; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane;

Reference yield:

: 134333-48-5
(E)-(2R,3R)-methyl 3-(dimethylphenylsilyl)-2-methoxyhex-4-enoate

: 134333-59-8
(2S,5S,6R)-6-(2,5-dimethoxyphenyl)-2,6-dimethoxy-1-hydroxy-5-methylhex-3-enyl-(E)-(1R)-acetylmandelic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / trimethylsilyl trifluoromethanesulfonate / CH₂Cl₂ / 6 h / -78 °C

2: LiAlH₄ / tetrahydrofuran / 0.25 h / 0 °C

3: DMAP, 1,3-dicyclohexylcarbodiimide / CH₂Cl₂ / 8 h / Ambient temperature

With dmap; lithium aluminium tetrahydride; trimethylsilyl trifluoromethanesulfonate; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane;

Reference yield:

: 134333-47-4
(2S,5S,6R)-(E)-methyl 6-(2,5-dimethoxyphenyl)-2,6-dimethoxy-5-methylhex-3-enoate

: 134333-59-8
(2S,5S,6R)-6-(2,5-dimethoxyphenyl)-2,6-dimethoxy-1-hydroxy-5-methylhex-3-enyl-(E)-(1R)-acetylmandelic acid

Guidance literature:: Multi-step reaction with 2 steps

1: LiAlH₄ / tetrahydrofuran / 0.25 h / 0 °C

2: DMAP, 1,3-dicyclohexylcarbodiimide / CH₂Cl₂ / 8 h / Ambient temperature

With dmap; lithium aluminium tetrahydride; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane;