(2S,5S,6R)-(E)-methyl 6-(2,5-dimethoxyphenyl)-2,6-dimethoxy-5-methylhex-3-enoate

Base Information

Chemical Name:(2S,5S,6R)-(E)-methyl 6-(2,5-dimethoxyphenyl)-2,6-dimethoxy-5-methylhex-3-enoate
CAS No.:134333-47-4
Molecular Formula:C₁₈H₂₆O₆
Molecular Weight:338.401
Hs Code.:

Synonyms:(2S,5S,6R)-(E)-methyl 6-(2,5-dimethoxyphenyl)-2,6-dimethoxy-5-methylhex-3-enoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,5S,6R)-(E)-methyl 6-(2,5-dimethoxyphenyl)-2,6-dimethoxy-5-methylhex-3-enoate

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Technology Process of (2S,5S,6R)-(E)-methyl 6-(2,5-dimethoxyphenyl)-2,6-dimethoxy-5-methylhex-3-enoate

There total 1 articles about (2S,5S,6R)-(E)-methyl 6-(2,5-dimethoxyphenyl)-2,6-dimethoxy-5-methylhex-3-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 74327-86-9
α,α,2,5-tetramethoxytoluene

: 134333-48-5
(E)-(2R,3R)-methyl 3-(dimethylphenylsilyl)-2-methoxyhex-4-enoate

: 134333-47-4
(2S,5S,6R)-(E)-methyl 6-(2,5-dimethoxyphenyl)-2,6-dimethoxy-5-methylhex-3-enoate

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -78 ℃; for 6h;

Reference yield:

: 134333-47-4
(2S,5S,6R)-(E)-methyl 6-(2,5-dimethoxyphenyl)-2,6-dimethoxy-5-methylhex-3-enoate

: 143470-39-7
(E)-(2S,5S,6R)-6-(2,5-Dimethoxy-phenyl)-2,6-dimethoxy-5-methyl-hex-3-en-1-ol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 0.25h;

Reference yield:

: 134333-47-4
(2S,5S,6R)-(E)-methyl 6-(2,5-dimethoxyphenyl)-2,6-dimethoxy-5-methylhex-3-enoate

: 134333-59-8
(2S,5S,6R)-6-(2,5-dimethoxyphenyl)-2,6-dimethoxy-1-hydroxy-5-methylhex-3-enyl-(E)-(1R)-acetylmandelic acid

Guidance literature:: Multi-step reaction with 2 steps

1: LiAlH₄ / tetrahydrofuran / 0.25 h / 0 °C

2: DMAP, 1,3-dicyclohexylcarbodiimide / CH₂Cl₂ / 8 h / Ambient temperature

With dmap; lithium aluminium tetrahydride; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane;