(5,10,15,20-tetratolylporphyrinato)(4-fluorobenzoyl)iridium(III) toluene

Base Information

Chemical Name:(5,10,15,20-tetratolylporphyrinato)(4-fluorobenzoyl)iridium(III) toluene
CAS No.:928267-48-5
Molecular Formula:C₇H₈*C₅₅H₄₀FIrN₄O
Molecular Weight:1076.31
Hs Code.:

Synonyms:(5,10,15,20-tetratolylporphyrinato)(4-fluorobenzoyl)iridium(III) toluene

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Chemical Property of (5,10,15,20-tetratolylporphyrinato)(4-fluorobenzoyl)iridium(III) toluene

Chemical Property:

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Technology Process of (5,10,15,20-tetratolylporphyrinato)(4-fluorobenzoyl)iridium(III) toluene

There total 2 articles about (5,10,15,20-tetratolylporphyrinato)(4-fluorobenzoyl)iridium(III) toluene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 872415-81-1
(5,10,15,20-tetrakis(p-tolyl)porphyrinato)carbonyliridium(III) chloride

: 459-57-4
4-fluorobenzaldehyde

: 108-88-3,15644-74-3,16713-13-6
toluene

: 928267-48-5
(5,10,15,20-tetratolylporphyrinato)(4-fluorobenzoyl)iridium(III) toluene

Guidance literature:: With 2,6-di-tert-butylpyridine; In neat (no solvent); (N2); dark; Ir complex (and pyridine (10 equiv.)) was dissolved in aldehyde; mixt. was heated at 200°C for 15 h; distd. (vac.); chromd. (silica gel, hexane/CH2Cl2, 2/1); recrystd. (CH2Cl2/MeOH); elem. anal.;
DOI:10.1021/om060849+

Reference yield: 88.0%

: 386707-40-0
(5,10,15,20-tetrakis(p-tolyl)porphyrinato)(methyl)iridium(III)

: 459-57-4
4-fluorobenzaldehyde

: 108-88-3,15644-74-3,16713-13-6
toluene

: 928267-48-5
(5,10,15,20-tetratolylporphyrinato)(4-fluorobenzoyl)iridium(III) toluene

Guidance literature:: In neat (no solvent); (N2); dark; suspn. of Ir complex and aldehyde was heated at 200°Cfor 1.5 h; chromd. (silica gel, hexane/CH2Cl2, 2/1);
DOI:10.1021/om060849+