C₃₁H₄₆O₅Si

Base Information

Chemical Name:C₃₁H₄₆O₅Si
CAS No.:938455-33-5
Molecular Formula:C₃₁H₄₆O₅Si
Molecular Weight:526.789
Hs Code.:

C<sub>31</sub>H<sub>46</sub>O<sub>5</sub>Si

Synonyms:C₃₁H₄₆O₅Si

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Chemical Property of C₃₁H₄₆O₅Si

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Technology Process of C₃₁H₄₆O₅Si

There total 12 articles about C₃₁H₄₆O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 938455-98-2
C₂₅H₃₄O₅(SiC₆H₁₄)

: 938455-33-5
C₃₁H₄₆O₅Si

Guidance literature:: With pyridine-SO₃ complex; dimethyl sulfoxide; triethylamine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1002/anie.200604625

Reference yield:

: 100-39-0
benzyl bromide

: 938455-33-5
C₃₁H₄₆O₅Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: NaH / dimethylformamide / 1.5 h / 0 °C

1.2: Bu₄NI / dimethylformamide / 15 h / 20 °C

2.1: 3.95 g / p-TsOH*H₂O / methanol / 3 h / 40 - 70 °C

3.1: 2,6-lutidine / CH₂Cl₂ / 1.5 h / 20 °C

4.1: 4.77 g / CSA / CH₂Cl₂; methanol / 2 h / 0 °C

5.1: 94 percent / Et₃N; SO₃*pyridine / CH₂Cl₂; dimethylsulfoxide / 2.5 h / 20 °C / Parikh-Doering oxidation

With 2,6-dimethylpyridine; pyridine-SO₃ complex; camphor-10-sulfonic acid; sodium hydride; toluene-4-sulfonic acid; triethylamine; In methanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2007.02.039

Reference yield:

: 938455-96-0
C₂₅H₃₂O₅

: 938455-33-5
C₃₁H₄₆O₅Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: NaH / dimethylformamide / 1.5 h / 0 °C

1.2: Bu₄NI / dimethylformamide / 15 h / 20 °C

2.1: 3.95 g / p-TsOH*H₂O / methanol / 3 h / 40 - 70 °C

3.1: 2,6-lutidine / CH₂Cl₂ / 1.5 h / 20 °C

4.1: 4.77 g / CSA / CH₂Cl₂; methanol / 2 h / 0 °C

5.1: 94 percent / Et₃N; SO₃*pyridine / CH₂Cl₂; dimethylsulfoxide / 2.5 h / 20 °C / Parikh-Doering oxidation

With 2,6-dimethylpyridine; pyridine-SO₃ complex; camphor-10-sulfonic acid; sodium hydride; toluene-4-sulfonic acid; triethylamine; In methanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2007.02.039