3-chloro-α-methylstyrene oxide

Base Information

Chemical Name:3-chloro-α-methylstyrene oxide
CAS No.:1427715-40-9
Molecular Formula:C₉H₉ClO
Molecular Weight:168.623
Hs Code.:

Synonyms:3-chloro-α-methylstyrene oxide

Suppliers and Price of 3-chloro-α-methylstyrene oxide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 3-chloro-α-methylstyrene oxide

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of 3-chloro-α-methylstyrene oxide

There total 3 articles about 3-chloro-α-methylstyrene oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 2-(3-chlorophenyl)propane-1,2-diol

: 1427715-40-9
3-chloro-α-methylstyrene oxide

Guidance literature:: With dmap; triethylamine; p-toluenesulfonyl chloride; In dichloromethane; at 0 - 50 ℃; for 24h; Inert atmosphere;
DOI:10.1039/c7cc06745c

Reference yield:

: 99-02-5
3'-Chloroacetophenone

: 1427715-40-9
3-chloro-α-methylstyrene oxide

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / tetrahydrofuran / 1 h / Reflux

1.2: Wittig Olefination / 0 °C / Reflux

2.1: 9-(2-mesityl)-10-methylacridinium perchlorate; sodium hydrogencarbonate / acetonitrile / 6 h / 20 °C / Irradiation

2.2: 3 h / 20 °C

3.1: triethylamine; p-toluenesulfonyl chloride; dmap / dichloromethane / 24 h / 0 - 50 °C / Inert atmosphere

With dmap; sodium hydride; sodium hydrogencarbonate; triethylamine; p-toluenesulfonyl chloride; 9-(2-mesityl)-10-methylacridinium perchlorate; In tetrahydrofuran; dichloromethane; acetonitrile; 1.1: |Wittig Olefination;
DOI:10.1039/c7cc06745c

Reference yield:

: 1712-71-6
3-chloro-α-methylstyrene

: 1427715-40-9
3-chloro-α-methylstyrene oxide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 9-(2-mesityl)-10-methylacridinium perchlorate; sodium hydrogencarbonate / acetonitrile / 6 h / 20 °C / Irradiation

1.2: 3 h / 20 °C

2.1: triethylamine; p-toluenesulfonyl chloride; dmap / dichloromethane / 24 h / 0 - 50 °C / Inert atmosphere

With dmap; sodium hydrogencarbonate; triethylamine; p-toluenesulfonyl chloride; 9-(2-mesityl)-10-methylacridinium perchlorate; In dichloromethane; acetonitrile;
DOI:10.1039/c7cc06745c