(Z)-6-N-(4-tert-butylbenzoyl)-9-[2-(dimethoxytrityloxymethyl)-3-hydroxyprop-1-enyl]adenine

Base Information

• Chemical Name: (Z)-6-N-(4-tert-butylbenzoyl)-9-[2-(dimethoxytrityloxymethyl)-3-hydroxyprop-1-enyl]adenine
• CAS No.: 885007-83-0
• Molecular Formula: C₄₁H₄₁N₅O₅
• Molecular Weight: 683.807

Synonyms:(Z)-6-N-(4-tert-butylbenzoyl)-9-[2-(dimethoxytrityloxymethyl)-3-hydroxyprop-1-enyl]adenine

Chemical Property of (Z)-6-N-(4-tert-butylbenzoyl)-9-[2-(dimethoxytrityloxymethyl)-3-hydroxyprop-1-enyl]adenine

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Technology Process of (Z)-6-N-(4-tert-butylbenzoyl)-9-[2-(dimethoxytrityloxymethyl)-3-hydroxyprop-1-enyl]adenine

There total 1 articles about (Z)-6-N-(4-tert-butylbenzoyl)-9-[2-(dimethoxytrityloxymethyl)-3-hydroxyprop-1-enyl]adenine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

4,4'-dimethoxytrityl chloride (40615-36-9) + N-6-(4-tert-butylbenzoyl)-9-[3-hydroxy-2-(hydroxymethyl)prop-1-enyl]adenine (705254-53-1) → C62H59N5O7 + (E)-6-N-(4-tert-butylbenzoyl)-9-[2-(dimethoxytrityloxymethyl)-3-hydroxyprop-1-enyl]adenine + (Z)-6-N-(4-tert-butylbenzoyl)-9-[2-(dimethoxytrityloxymethyl)-3-hydroxyprop-1-enyl]adenine (885007-83-0)

Guidance literature:

With pyridine; at 20 ℃; for 3h;

DOI:10.1039/b517504f

Reference yield: 72.0%

(Z)-6-N-(4-tert-butylbenzoyl)-9-[2-(dimethoxytrityloxymethyl)-3-hydroxyprop-1-enyl]adenine (885007-83-0) + 2-cyanoethyl-N,N-(diisopropylamino)chlorophosphine (124482-92-4,89992-70-1) → (E)-9-[3-(dimethoxytrityloxy)-2-[2-cyanoethoxy(diisopropylamino)phosphinoxymethyl]prop-1-enyl]-N-6-(4-tert-butylbenzoyl)adenine

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃; for 2h;

DOI:10.1039/b517504f

Reference yield: 70.0%

(Z)-6-N-(4-tert-butylbenzoyl)-9-[2-(dimethoxytrityloxymethyl)-3-hydroxyprop-1-enyl]adenine (885007-83-0) + O-[2-[N-methyl-N-(2-pyridyl)amino]ethyl] N,N,N',N'-tetraisopropylphosphorodiamidite (650599-81-8) → (E)-1-[3-(dimethoxytrityloxy)-2-[{N-methyl-N-(2-pyridyl)-2-aminoethoxy}(diisopropylamino)phosphinoxymethyl]prop-1-enyl]-N-6-(4-tert-butylbenzoyl)adenine

Guidance literature:

With 1H-tetrazole; In acetonitrile; at 20 ℃; for 2h;

DOI:10.1039/b517504f

upstream raw materials:

4,4'-dimethoxytrityl chloride

N-6-(4-tert-butylbenzoyl)-9-[3-hydroxy-2-(hydroxymethyl)prop-1-enyl]adenine

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