3-nitro-5-vinyl phenol

Base Information

Chemical Name:3-nitro-5-vinyl phenol
CAS No.:1447811-39-3
Molecular Formula:C₈H₇NO₃
Molecular Weight:165.148
Hs Code.:

Synonyms:3-nitro-5-vinyl phenol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-nitro-5-vinyl phenol

Chemical Property:

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Technology Process of 3-nitro-5-vinyl phenol

There total 3 articles about 3-nitro-5-vinyl phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 116632-23-6
3-bromo-5-nitro-phenol

: potassium vinyltrifluoroborate

: 1447811-39-3
3-nitro-5-vinyl phenol

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; potassium carbonate; triphenylphosphine; In tetrahydrofuran; water; at 100 ℃; for 16h; Inert atmosphere;
DOI:10.1021/ja4061273

Reference yield:

: 915156-09-1
2-amino-3-bromo-5-nitro-phenol

: 1447811-39-3
3-nitro-5-vinyl phenol

Guidance literature:: Multi-step reaction with 2 steps

1.1: sulfuric acid / ethanol / 0.5 h

1.2: 3.5 h / Reflux

2.1: triethylamine; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / tetrahydrofuran; isopropyl alcohol / 12 h / Inert atmosphere; Reflux; Sealed tube

With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; sulfuric acid; triethylamine; In tetrahydrofuran; ethanol; isopropyl alcohol;

Reference yield:

: 121-88-0
5-Nitro-2-aminophenol

: 1447811-39-3
3-nitro-5-vinyl phenol

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-Bromosuccinimide / acetonitrile / 2 h / 20 °C

2.1: sulfuric acid / ethanol / 0.5 h

2.2: 3.5 h / Reflux

3.1: triethylamine; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / tetrahydrofuran; isopropyl alcohol / 12 h / Inert atmosphere; Reflux; Sealed tube

With N-Bromosuccinimide; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; sulfuric acid; triethylamine; In tetrahydrofuran; ethanol; isopropyl alcohol; acetonitrile;