Technology Process of 3-nitro-5-vinyl phenol
There total 3 articles about 3-nitro-5-vinyl phenol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
bis-triphenylphosphine-palladium(II) chloride; potassium carbonate; triphenylphosphine;
In
tetrahydrofuran; water;
at 100 ℃;
for 16h;
Inert atmosphere;
DOI:10.1021/ja4061273
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sulfuric acid / ethanol / 0.5 h
1.2: 3.5 h / Reflux
2.1: triethylamine; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2 / tetrahydrofuran; isopropyl alcohol / 12 h / Inert atmosphere; Reflux; Sealed tube
With
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; sulfuric acid; triethylamine;
In
tetrahydrofuran; ethanol; isopropyl alcohol;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: N-Bromosuccinimide / acetonitrile / 2 h / 20 °C
2.1: sulfuric acid / ethanol / 0.5 h
2.2: 3.5 h / Reflux
3.1: triethylamine; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2 / tetrahydrofuran; isopropyl alcohol / 12 h / Inert atmosphere; Reflux; Sealed tube
With
N-Bromosuccinimide; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; sulfuric acid; triethylamine;
In
tetrahydrofuran; ethanol; isopropyl alcohol; acetonitrile;
