{Fe(TPP)(py)2}ClO₄*2THF

Base Information

• Chemical Name: {Fe(TPP)(py)2}ClO₄*2THF
• CAS No.: 115269-81-3
• Molecular Formula: 2C₄H₈O*C₅₄H₃₈FeN₆*ClO₄
• Molecular Weight: 1070.45
• Mol file: 115269-81-3.mol

Synonyms:{Fe(TPP)(py)2}ClO₄*2THF

Chemical Property of {Fe(TPP)(py)2}ClO₄*2THF

Chemical Property:

Purity/Quality:

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Technology Process of {Fe(TPP)(py)2}ClO₄*2THF

There total 2 articles about {Fe(TPP)(py)2}ClO₄*2THF which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

pyridine (110-86-1) + {Fe(TPP)(H2O)2}ClO4*2THF → {Fe(TPP)(py)2}ClO4*2THF (115269-81-3)

Guidance literature:

With HClO₄; In tetrahydrofuran; soln. of {Fe(TPP)(H2O)2}ClO4*2THF in THF, addn. of pyridine and HClO4, stirring (1 h), evapn. to vol. of 4 ml; heptane vapor diffusion; elem. anal.;

DOI:10.1021/ja00225a010

Reference yield:

chloro[5,10,15,20-tetraphenylporphyrinato]iron(III) → {Fe(TPP)(py)2}ClO4*2THF (115269-81-3)

Guidance literature:

Multi-step reaction with 2 steps

1: not given

2: HClO₄ / tetrahydrofuran

With HClO₄; In tetrahydrofuran;

DOI:10.1021/ja00225a010

upstream raw materials:

pyridine