C₁₄H₁₃BrFN₃

Base Information

Chemical Name:C₁₄H₁₃BrFN₃
CAS No.:1262197-58-9
Molecular Formula:C₁₄H₁₃BrFN₃
Molecular Weight:322.18
Hs Code.:

C<sub>14</sub>H<sub>13</sub>BrFN<sub>3</sub>

Synonyms:C₁₄H₁₃BrFN₃

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Chemical Property of C₁₄H₁₃BrFN₃

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Technology Process of C₁₄H₁₃BrFN₃

There total 1 articles about C₁₄H₁₃BrFN₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: Tebbe's reagent

: 1262197-57-8
C₁₃H₁₁BrFN₃O

: 1262197-58-9
C₁₄H₁₃BrFN₃

Guidance literature:: In tetrahydrofuran; for 18h;

Reference yield: 69.0%

: 1262197-58-9
C₁₄H₁₃BrFN₃

: 1262197-59-0
C₁₂H₉BrFN₃

Guidance literature:: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In 1,2-dichloro-ethane; at 60 ℃; for 2h;

Reference yield:

: 1262197-58-9
C₁₄H₁₃BrFN₃

: 1314787-21-7
[8-(4-Fluoro-phenyl)-5,6,7,8-tetrahydro-[1,2,4]triazolo[1,5-a]pyridin-2-yl]-[3-methoxy-4-(2-methyl-pyridin-4-yl)-phenyl]-amine

Guidance literature:: Multi-step reaction with 3 steps

1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / 1,2-dichloro-ethane / 2 h / 60 °C

2: sodium tetrahydroborate; methanol / 2 h / 20 °C

3: caesium carbonate / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; XPhos / tert-butyl alcohol / 20 h / 110 °C / Inert atmosphere

With methanol; sodium tetrahydroborate; caesium carbonate; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; XPhos; In 1,2-dichloro-ethane; tert-butyl alcohol;