3-C-(O-(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-(1->4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)propene

Base Information

• Chemical Name: 3-C-(O-(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-(1->4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)propene
• CAS No.: 1097188-64-1
• Molecular Formula: C₅₁H₅₀N₂O₁₅
• Molecular Weight: 930.962

Synonyms:3-C-(O-(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-(1->4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)propene

Chemical Property of 3-C-(O-(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-(1->4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)propene

Chemical Property:

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Technology Process of 3-C-(O-(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-(1->4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)propene

There total 2 articles about 3-C-(O-(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-(1->4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)propene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

3-C-(3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)propene (1097188-65-2) + 3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl-O-trichloroacetimidate (87190-67-8) → 3-C-(O-(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-(1->4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)propene (1097188-64-1)

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -30 ℃; for 2h; Inert atmosphere; Molecular sieve;

DOI:10.1021/jo801906s

Reference yield: 45.0%

3-C-(3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)propene (1097188-65-2) + phenyl 3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside (79528-49-7) → 3-C-(O-(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-(1->4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)propene (1097188-64-1)

Guidance literature:

With trifluoromethylsulfonic anhydride; 1,1'-sulfinylbisbenzene; Inert atmosphere;

DOI:10.1021/jo801906s

Reference yield:

3-C-(O-(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-(1->4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)propene (1097188-64-1) → C35H46N2O11

Guidance literature:

With ethylenediamine; In butan-1-ol; at 90 ℃; Inert atmosphere; Molecular sieve;

DOI:10.1021/jo801906s

upstream raw materials:

3-C-(3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)propene

3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl-O-trichloroacetimidate

phenyl 3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

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