4-(2-benzyloxyethyl)phenyl 2,4,6-tri-O-acetyl-3-O-[4-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyl)benzyl]-β-D-glucopyranoside

Base Information

Chemical Name:4-(2-benzyloxyethyl)phenyl 2,4,6-tri-O-acetyl-3-O-[4-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyl)benzyl]-β-D-glucopyranoside
CAS No.:1338932-23-2
Molecular Formula:C₄₅H₄₃F₁₇O₁₀
Molecular Weight:1066.8
Hs Code.:

Synonyms:4-(2-benzyloxyethyl)phenyl 2,4,6-tri-O-acetyl-3-O-[4-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyl)benzyl]-β-D-glucopyranoside

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Chemical Property of 4-(2-benzyloxyethyl)phenyl 2,4,6-tri-O-acetyl-3-O-[4-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyl)benzyl]-β-D-glucopyranoside

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Technology Process of 4-(2-benzyloxyethyl)phenyl 2,4,6-tri-O-acetyl-3-O-[4-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyl)benzyl]-β-D-glucopyranoside

There total 1 articles about 4-(2-benzyloxyethyl)phenyl 2,4,6-tri-O-acetyl-3-O-[4-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyl)benzyl]-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 204971-31-3
4-{2-[(phenylmethyl)oxy]ethyl}phenol

: C₃₂H₂₉Cl₃F₁₇NO₉

: 1338932-23-2
4-(2-benzyloxyethyl)phenyl 2,4,6-tri-O-acetyl-3-O-[4-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyl)benzyl]-β-D-glucopyranoside

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at -20 ℃; for 1h; Molecular sieve;
DOI:10.1016/j.tet.2011.08.087

Reference yield:

: 1338932-23-2
4-(2-benzyloxyethyl)phenyl 2,4,6-tri-O-acetyl-3-O-[4-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyl)benzyl]-β-D-glucopyranoside

: 1338932-25-4
4-(2-benzyloxyethyl)phenyl 3-O-[4-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyl)benzyl]-β-D-glucopyranoside

Guidance literature:: With sodium methylate; In tetrahydrofuran; methanol; at 20 ℃; for 12h;
DOI:10.1016/j.tet.2011.08.087

Reference yield:

: 1338932-23-2
4-(2-benzyloxyethyl)phenyl 2,4,6-tri-O-acetyl-3-O-[4-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyl)benzyl]-β-D-glucopyranoside

: 1338932-27-6
4-(2-benzyloxyethyl)phenyl 4,6-O-benzylidene-3-O-[4-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyl)benzyl]-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: sodium methylate / tetrahydrofuran; methanol / 12 h / 20 °C

2: toluene-4-sulfonic acid / N,N-dimethyl-formamide / 3 h / 60 °C / Low pressure

With sodium methylate; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2011.08.087