(5Z)-3-benzyloxycarbonyl-2-(benzylsulfanyl)-5-(4-methoxybenzylidene)-4,5-dihydro-1H-imidazol-4-one

Base Information

Chemical Name:(5Z)-3-benzyloxycarbonyl-2-(benzylsulfanyl)-5-(4-methoxybenzylidene)-4,5-dihydro-1H-imidazol-4-one
CAS No.:1356003-62-7
Molecular Formula:C₂₆H₂₂N₂O₄S
Molecular Weight:458.538
Hs Code.:

Synonyms:(5Z)-3-benzyloxycarbonyl-2-(benzylsulfanyl)-5-(4-methoxybenzylidene)-4,5-dihydro-1H-imidazol-4-one

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Chemical Property of (5Z)-3-benzyloxycarbonyl-2-(benzylsulfanyl)-5-(4-methoxybenzylidene)-4,5-dihydro-1H-imidazol-4-one

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Technology Process of (5Z)-3-benzyloxycarbonyl-2-(benzylsulfanyl)-5-(4-methoxybenzylidene)-4,5-dihydro-1H-imidazol-4-one

There total 4 articles about (5Z)-3-benzyloxycarbonyl-2-(benzylsulfanyl)-5-(4-methoxybenzylidene)-4,5-dihydro-1H-imidazol-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 385797-51-3
(5Z)-2-(benzylsulfanyl)-5-(4-methoxybenzylidene)-4,5-dihydro-1H-imidazol-4-one

: 501-53-1,94274-21-2
benzyl chloroformate

: 1356003-62-7
(5Z)-3-benzyloxycarbonyl-2-(benzylsulfanyl)-5-(4-methoxybenzylidene)-4,5-dihydro-1H-imidazol-4-one

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1055/s-0030-1260259

Reference yield:

: 1356003-46-7
1-acetyl-2-(benzylsulfanyl)-4,5-dihydro-1H-imidazol-4-one

: 1356003-62-7
(5Z)-3-benzyloxycarbonyl-2-(benzylsulfanyl)-5-(4-methoxybenzylidene)-4,5-dihydro-1H-imidazol-4-one

Guidance literature:: Multi-step reaction with 4 steps

1: sodium methylate / methanol / 0 - 20 °C / pH 10 / Inert atmosphere; Molecular sieve

2: dmap / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

3: sodium acetate; acetic acid / Reflux

4: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

With dmap; sodium methylate; sodium acetate; acetic acid; triethylamine; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1055/s-0030-1260259

Reference yield:

: 95474-45-6,1809028-84-9
5-p-methoxybenzylidene-2-thiohydantoin

: 1356003-62-7
(5Z)-3-benzyloxycarbonyl-2-(benzylsulfanyl)-5-(4-methoxybenzylidene)-4,5-dihydro-1H-imidazol-4-one

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate / dichloromethane / 2 h / 20 °C / Inert atmosphere

2: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

With sodium hydrogencarbonate; triethylamine; In dichloromethane;
DOI:10.1055/s-0030-1260259