ethyl (6S)-3-O-benzyl-6-deoxy-6-(N-benzylaminomethyl)-1,2-O-isopropylidene-α-D-gluco-1,4-hepto-furanoate

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Chemical Name:ethyl (6S)-3-O-benzyl-6-deoxy-6-(N-benzylaminomethyl)-1,2-O-isopropylidene-α-D-gluco-1,4-hepto-furanoate
CAS No.:1225441-89-3
Molecular Formula:C₂₇H₃₅NO₇
Molecular Weight:485.577
Hs Code.:

Synonyms:ethyl (6S)-3-O-benzyl-6-deoxy-6-(N-benzylaminomethyl)-1,2-O-isopropylidene-α-D-gluco-1,4-hepto-furanoate

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Chemical Property of ethyl (6S)-3-O-benzyl-6-deoxy-6-(N-benzylaminomethyl)-1,2-O-isopropylidene-α-D-gluco-1,4-hepto-furanoate

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Technology Process of ethyl (6S)-3-O-benzyl-6-deoxy-6-(N-benzylaminomethyl)-1,2-O-isopropylidene-α-D-gluco-1,4-hepto-furanoate

There total 1 articles about ethyl (6S)-3-O-benzyl-6-deoxy-6-(N-benzylaminomethyl)-1,2-O-isopropylidene-α-D-gluco-1,4-hepto-furanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.7%

: 1225441-87-1
ethyl 3-O-benzyl-6-deoxy-6-methylene-1,2-O-isopropylidene-α-D-gluco-1,4-hepto-furanoate

: 100-46-9
benzylamine

: 1225441-89-3
ethyl (6S)-3-O-benzyl-6-deoxy-6-(N-benzylaminomethyl)-1,2-O-isopropylidene-α-D-gluco-1,4-hepto-furanoate

Guidance literature:: at 20 ℃; for 6h; Inert atmosphere;
DOI:10.1016/j.tet.2010.02.044

Reference yield: 86.0%

: 75-44-5
phosgene

: 1225441-89-3
ethyl (6S)-3-O-benzyl-6-deoxy-6-(N-benzylaminomethyl)-1,2-O-isopropylidene-α-D-gluco-1,4-hepto-furanoate

: 1225441-90-6
(6S)-3-O-benzyl-6,7-dideoxy-7-benzylamino-6-carboethoxy-[7-N,5-O-carbonyl]-α-D-gluco-1,4-hepto-furanose

Guidance literature:: With triethylamine; In toluene; at 0 ℃; for 0.166667h; Inert atmosphere;
DOI:10.1016/j.tet.2010.02.044

Reference yield: 67.0%

: 1225441-89-3
ethyl (6S)-3-O-benzyl-6-deoxy-6-(N-benzylaminomethyl)-1,2-O-isopropylidene-α-D-gluco-1,4-hepto-furanoate

: 1225441-92-8
(6R)-3-O-benzyl-6-deoxy-6-(N-benzylaminomethyl)-1,2-O-isopropylidene-α-D-gluco-1,4-hepto-furanose

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 - 20 ℃; for 2h; Inert atmosphere;
DOI:10.1016/j.tet.2010.02.044