Technology Process of C58H56N2O6
There total 5 articles about C58H56N2O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
2-(2-trityloxyethoxy)ethanol;
With
sodium hydride;
In
tetrahydrofuran;
for 3h;
Heating;
4,4'-bis(bromomethyl)-2,2'-bipyridine;
In
tetrahydrofuran;
at 30 ℃;
for 48h;
Further stages.;
DOI:10.1021/ja068707u
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 50 percent / aq. H2SO4; KMnO4 / 12 h / Heating
2.1: 99 percent / conc. H2SO4 / 60 h / Heating
3.1: 30 percent / NaBH4 / methanol / 60 h / Heating
4.1: 30 percent / aq. HBr / 3.5 h / Heating
5.1: NaH / tetrahydrofuran / 3 h / Heating
5.2: tetrahydrofuran / 48 h / 30 °C
With
sodium tetrahydroborate; potassium permanganate; sulfuric acid; hydrogen bromide; sodium hydride;
In
tetrahydrofuran; methanol;
DOI:10.1021/ja068707u
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 99 percent / conc. H2SO4 / 60 h / Heating
2.1: 30 percent / NaBH4 / methanol / 60 h / Heating
3.1: 30 percent / aq. HBr / 3.5 h / Heating
4.1: NaH / tetrahydrofuran / 3 h / Heating
4.2: tetrahydrofuran / 48 h / 30 °C
With
sodium tetrahydroborate; sulfuric acid; hydrogen bromide; sodium hydride;
In
tetrahydrofuran; methanol;
DOI:10.1021/ja068707u