ammonium 2-(benzyloxycarbonylamino)ethyl 2,2,2-trichloroethyl phosphate

Base Information

• Chemical Name: ammonium 2-(benzyloxycarbonylamino)ethyl 2,2,2-trichloroethyl phosphate
• CAS No.: 119220-17-6
• Molecular Formula: C₁₂H₁₅Cl₃NO₆P*H₃N
• Molecular Weight: 423.617

Synonyms:ammonium 2-(benzyloxycarbonylamino)ethyl 2,2,2-trichloroethyl phosphate

Chemical Property of ammonium 2-(benzyloxycarbonylamino)ethyl 2,2,2-trichloroethyl phosphate

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Technology Process of ammonium 2-(benzyloxycarbonylamino)ethyl 2,2,2-trichloroethyl phosphate

There total 1 articles about ammonium 2-(benzyloxycarbonylamino)ethyl 2,2,2-trichloroethyl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

2-(benzyloxycarbonylamino)ethyl 2,2,2-trichloroethyl morpholinophosphate (119220-13-2) → ammonium 2-(benzyloxycarbonylamino)ethyl 2,2,2-trichloroethyl phosphate (119220-17-6)

Guidance literature:

With ammonium hydroxide; Amberlite IR 77 (H+) resin; In methanol; water; at 60 ℃; for 10h;

Reference yield:

3,4,6-tri-O-acetyl-2-amino-2-deoxy-α-D-glucopyranosyl bromide hydrobromide (4710-88-7) + ammonium 2-(benzyloxycarbonylamino)ethyl 2,2,2-trichloroethyl phosphate (119220-17-6) + (3R)-3-acetoxytetradecanoic anhydride (85065-43-6) → 2-<(3R)-3-acetoxytertadecanamido>-3,4-6-tri-O-acetyl-2-deoxy-α-D-glucopyranosyl 2-(benzyloxycarbonylamino)ethyl 2,2,2-trichloroethyl phosphate (119220-21-2)

Guidance literature:

With triethylamine; Yield given. Multistep reaction; 1.) MeOH, H₂O; 2.) CHCl₃, 1 h; 3.) CHCl₃, EtOAc, 1 h;

Reference yield:

3,4,6-tri-O-acetyl-2-amino-2-deoxy-α-D-glucopyranosyl bromide hydrobromide (4710-88-7) + benzyl chloroformate (501-53-1,94274-21-2) + ammonium 2-(benzyloxycarbonylamino)ethyl 2,2,2-trichloroethyl phosphate (119220-17-6) → 2-(benzyloxycarbonylamino)ethyl 3,4,6-tri-O-acetyl-2-benzyloxycarbonylamino-2-deoxy-α-D-glucopyranosyl 2,2,2-trichloroethyl phosphate (119220-18-7)

Guidance literature:

With triethylamine; Yield given. Multistep reaction; 1.) MeOH, H₂O; 2.) CHCl₃, 1 h; 3.) pyridine, toluene, 25 min;

upstream raw materials:

2-(benzyloxycarbonylamino)ethyl 2,2,2-trichloroethyl morpholinophosphate

Downstream raw materials:

2-<(3R)-3-acetoxytertadecanamido>-3,4-6-tri-O-acetyl-2-deoxy-α-D-glucopyranosyl 2-(benzyloxycarbonylamino)ethyl 2,2,2-trichloroethyl phosphate

2-(benzyloxycarbonylamino)ethyl 3,4,6-tri-O-acetyl-2-benzyloxycarbonylamino-2-deoxy-α-D-glucopyranosyl 2,2,2-trichloroethyl phosphate

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