2-(benzyloxycarbonylamino)ethyl 2,2,2-trichloroethyl morpholinophosphate

Base Information

Chemical Name:2-(benzyloxycarbonylamino)ethyl 2,2,2-trichloroethyl morpholinophosphate
CAS No.:119220-13-2
Molecular Formula:C₁₆H₂₂Cl₃N₂O₆P
Molecular Weight:475.693
Hs Code.:

Synonyms:2-(benzyloxycarbonylamino)ethyl 2,2,2-trichloroethyl morpholinophosphate

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Chemical Property of 2-(benzyloxycarbonylamino)ethyl 2,2,2-trichloroethyl morpholinophosphate

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Technology Process of 2-(benzyloxycarbonylamino)ethyl 2,2,2-trichloroethyl morpholinophosphate

There total 1 articles about 2-(benzyloxycarbonylamino)ethyl 2,2,2-trichloroethyl morpholinophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 77987-49-6
benzyl 2-hydroxyethylcarbamate

: 119220-12-1
2,2,2-trichloroethyl 4-morpholinylphosphonochloridate

: 119220-13-2
2-(benzyloxycarbonylamino)ethyl 2,2,2-trichloroethyl morpholinophosphate

Guidance literature:: With dmap; In pyridine; for 16h;

Reference yield: 59.0%

: 119220-13-2
2-(benzyloxycarbonylamino)ethyl 2,2,2-trichloroethyl morpholinophosphate

: 119220-17-6
ammonium 2-(benzyloxycarbonylamino)ethyl 2,2,2-trichloroethyl phosphate

Guidance literature:: With ammonium hydroxide; Amberlite IR 77 (H+) resin; In methanol; water; at 60 ℃; for 10h;

Reference yield:

: 119220-13-2
2-(benzyloxycarbonylamino)ethyl 2,2,2-trichloroethyl morpholinophosphate

: 119220-18-7
2-(benzyloxycarbonylamino)ethyl 3,4,6-tri-O-acetyl-2-benzyloxycarbonylamino-2-deoxy-α-D-glucopyranosyl 2,2,2-trichloroethyl phosphate

Guidance literature:: Multi-step reaction with 2 steps

1: 59 percent / 1.) Amberlite IR 77 (H+) resin, 2.) 1 M aq.NH₄OH / H₂O; methanol / 10 h / 60 °C

2: 1.) Et₃N, 2.) Et₃N / 1.) MeOH, H₂O; 2.) CHCl₃, 1 h; 3.) pyridine, toluene, 25 min

With ammonium hydroxide; Amberlite IR 77 (H+) resin; triethylamine; In methanol; water;