5-benzyl-5-phenylselenenyl-2',3'-O-isopropylidene-5'-O-methoxymethyluridine

Base Information

Chemical Name:5-benzyl-5-phenylselenenyl-2',3'-O-isopropylidene-5'-O-methoxymethyluridine
CAS No.:99388-45-1
Molecular Formula:C₂₇H₃₂N₂O₇Se
Molecular Weight:575.52
Hs Code.:

Synonyms:5-benzyl-5-phenylselenenyl-2',3'-O-isopropylidene-5'-O-methoxymethyluridine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-benzyl-5-phenylselenenyl-2',3'-O-isopropylidene-5'-O-methoxymethyluridine

Chemical Property:

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Technology Process of 5-benzyl-5-phenylselenenyl-2',3'-O-isopropylidene-5'-O-methoxymethyluridine

There total 5 articles about 5-benzyl-5-phenylselenenyl-2',3'-O-isopropylidene-5'-O-methoxymethyluridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 362-43-6
2',3'-O-isopropylideneuridine

: 99388-45-1
5-benzyl-5-phenylselenenyl-2',3'-O-isopropylidene-5'-O-methoxymethyluridine

Guidance literature:: Multi-step reaction with 4 steps

1: 90.4 percent / methanesulfonic acid / acetone / Ambient temperature

2: 99 percent / H₂ / 5percent Rh on alumina / methanol / 2 h / 760 Torr

3: 1.) LDA / 1.) THF, - 70 deg C, 1 h; 2.) THF, - 70 deg C, 2 h

4: 1.) LDA / 1.) THF; 2.) - 70 deg C, overnight

With methanesulfonic acid; hydrogen; lithium diisopropyl amide; rhodium on alumina; In methanol; acetone;
DOI:10.1016/S0040-4020(01)96481-6

Reference yield:

: 80614-78-4
2',3'-O-isopropylidene-5'-O-methoxymethyl-uridine

: 99388-45-1
5-benzyl-5-phenylselenenyl-2',3'-O-isopropylidene-5'-O-methoxymethyluridine

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / H₂ / 5percent Rh on alumina / methanol / 2 h / 760 Torr

2: 1.) LDA / 1.) THF, - 70 deg C, 1 h; 2.) THF, - 70 deg C, 2 h

3: 1.) LDA / 1.) THF; 2.) - 70 deg C, overnight

With hydrogen; lithium diisopropyl amide; rhodium on alumina; In methanol;
DOI:10.1016/S0040-4020(01)96481-6

Reference yield:

: 5707-04-0
Phenylselenyl chloride

: 99388-45-1
5-benzyl-5-phenylselenenyl-2',3'-O-isopropylidene-5'-O-methoxymethyluridine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) LDA / 1.) THF, - 70 deg C, 1 h; 2.) THF, - 70 deg C, 2 h

2: 1.) LDA / 1.) THF; 2.) - 70 deg C, overnight

With lithium diisopropyl amide;
DOI:10.1016/S0040-4020(01)96481-6