ethyl 1-benzoyl-2-acetamidomethyl-4-carbetoxyethylpyrrole-3-acetate

Base Information

Chemical Name:ethyl 1-benzoyl-2-acetamidomethyl-4-carbetoxyethylpyrrole-3-acetate
CAS No.:87721-26-4
Molecular Formula:C₂₃H₂₈N₂O₆
Molecular Weight:428.485
Hs Code.:

Synonyms:ethyl 1-benzoyl-2-acetamidomethyl-4-carbetoxyethylpyrrole-3-acetate

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Chemical Property of ethyl 1-benzoyl-2-acetamidomethyl-4-carbetoxyethylpyrrole-3-acetate

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Technology Process of ethyl 1-benzoyl-2-acetamidomethyl-4-carbetoxyethylpyrrole-3-acetate

There total 7 articles about ethyl 1-benzoyl-2-acetamidomethyl-4-carbetoxyethylpyrrole-3-acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 71616-57-4
ethyl 2-(3-pyrrolyl)acetate

: 87721-26-4
ethyl 1-benzoyl-2-acetamidomethyl-4-carbetoxyethylpyrrole-3-acetate

Guidance literature:: Multi-step reaction with 6 steps

1: 53 percent / CSI / CH₂Cl₂; acetonitrile / 2.5 h / -42 °C

2: 97 percent / iodic acid/iodine, conc. sulfuric acid / CCl₄; H₂O; acetic acid / 24 h / Ambient temperature

3: 99.5 percent / NaOH, tetrabutylammonium hydrogen sulfate / CH₂Cl₂ / 2 h / 0 °C

4: 31.2 percent / triethylamine, palladium(II) acetate / acetonitrile / 0.67 h / 99 - 100 °C

5: 91.5 percent / NaOH, tetrabutylammonium hydrogen sulfate / CH₂Cl₂ / 2 h / 0 °C

6: hydrogen / PtO₂ / 6 h / Ambient temperature

With sodium hydroxide; isocyanate de chlorosulfonyle; sulfuric acid; hydrogen; iodine; tetra(n-butyl)ammonium hydrogensulfate; palladium diacetate; iodic acid; triethylamine; platinum(IV) oxide; In tetrachloromethane; dichloromethane; water; acetic acid; acetonitrile;

Reference yield:

: 98-88-4
benzoyl chloride

: 87721-26-4
ethyl 1-benzoyl-2-acetamidomethyl-4-carbetoxyethylpyrrole-3-acetate

Guidance literature:: Multi-step reaction with 3 steps

1: 99.5 percent / NaOH, tetrabutylammonium hydrogen sulfate / CH₂Cl₂ / 2 h / 0 °C

2: 58 percent / triethylamine, palladium(II) acetate / acetonitrile / 0.67 h / 99 - 100 °C

3: hydrogen / PtO₂ / 6 h / Ambient temperature

With sodium hydroxide; hydrogen; tetra(n-butyl)ammonium hydrogensulfate; palladium diacetate; triethylamine; platinum(IV) oxide; In dichloromethane; acetonitrile;

Reference yield:

: 87721-19-5
ethyl 2-cyano-4-iodopyrrole-3-acetate

: 87721-26-4
ethyl 1-benzoyl-2-acetamidomethyl-4-carbetoxyethylpyrrole-3-acetate

Guidance literature:: Multi-step reaction with 4 steps

1: 99.5 percent / NaOH, tetrabutylammonium hydrogen sulfate / CH₂Cl₂ / 2 h / 0 °C

2: 31.2 percent / triethylamine, palladium(II) acetate / acetonitrile / 0.67 h / 99 - 100 °C

3: 91.5 percent / NaOH, tetrabutylammonium hydrogen sulfate / CH₂Cl₂ / 2 h / 0 °C

4: hydrogen / PtO₂ / 6 h / Ambient temperature

With sodium hydroxide; hydrogen; tetra(n-butyl)ammonium hydrogensulfate; palladium diacetate; triethylamine; platinum(IV) oxide; In dichloromethane; acetonitrile;