(S)-tert-butyl (1-(benzo[d]thiazol-2-yl)-1-oxo-3-phenylpropan-2-yl)carbamate

Base Information

Chemical Name:(S)-tert-butyl (1-(benzo[d]thiazol-2-yl)-1-oxo-3-phenylpropan-2-yl)carbamate
CAS No.:942129-04-6
Molecular Formula:C₂₁H₂₂N₂O₃S
Molecular Weight:382.483
Hs Code.:

Synonyms:(S)-tert-butyl (1-(benzo[d]thiazol-2-yl)-1-oxo-3-phenylpropan-2-yl)carbamate

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Chemical Property of (S)-tert-butyl (1-(benzo[d]thiazol-2-yl)-1-oxo-3-phenylpropan-2-yl)carbamate

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Technology Process of (S)-tert-butyl (1-(benzo[d]thiazol-2-yl)-1-oxo-3-phenylpropan-2-yl)carbamate

There total 4 articles about (S)-tert-butyl (1-(benzo[d]thiazol-2-yl)-1-oxo-3-phenylpropan-2-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 95-16-9
1,3-Benzothiazole

: 4522-04-7,53588-99-1
ethyl N-{[(1,1-dimethylethyl)oxy]carbonyl}-L-phenylalaninate

: 942129-04-6
(S)-tert-butyl (1-(benzo[d]thiazol-2-yl)-1-oxo-3-phenylpropan-2-yl)carbamate

Guidance literature:: 1,3-Benzothiazole; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h; Inert atmosphere;

ethyl N-{[(1,1-dimethylethyl)oxy]carbonyl}-L-phenylalaninate; In tetrahydrofuran; hexane; Inert atmosphere;
DOI:10.1016/j.bmcl.2016.01.087

Reference yield:

: 95-16-9
1,3-Benzothiazole

: C₂₂H₂₈N₄O₄

: 942129-04-6
(S)-tert-butyl (1-(benzo[d]thiazol-2-yl)-1-oxo-3-phenylpropan-2-yl)carbamate

Guidance literature:: 1,3-Benzothiazole; With TurboGrignard; In tetrahydrofuran; at -10 ℃; for 0.55h;

C₂₂H₂₈N₄O₄; In tetrahydrofuran; at -10 - 20 ℃; for 3h;
DOI:10.1016/j.tetlet.2019.05.043

Reference yield:

: 95-16-9
1,3-Benzothiazole

: 87694-53-9
Boc-Phe-OH N,O-dimethyl hydroxamate

: 942129-04-6
(S)-tert-butyl (1-(benzo[d]thiazol-2-yl)-1-oxo-3-phenylpropan-2-yl)carbamate

Guidance literature:: 1,3-Benzothiazole; With n-butyllithium; In tetrahydrofuran; hexane; at -70 ℃; for 0.5h;

Boc-Phe-OH N,O-dimethyl hydroxamate; In tetrahydrofuran; hexane; at -70 ℃; for 2h;
DOI:10.1021/jm0303857