[(S)-1,5,10,14-Tetrakis-(toluene-4-sulfonyl)-1,5,10,14-tetraaza-cyclooctadec-6-yl]-methanol

Base Information

Chemical Name:[(S)-1,5,10,14-Tetrakis-(toluene-4-sulfonyl)-1,5,10,14-tetraaza-cyclooctadec-6-yl]-methanol
CAS No.:109240-53-1
Molecular Formula:C₄₃H₅₈N₄O₉S₄
Molecular Weight:903.219
Hs Code.:

Synonyms:[(S)-1,5,10,14-Tetrakis-(toluene-4-sulfonyl)-1,5,10,14-tetraaza-cyclooctadec-6-yl]-methanol

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Chemical Property of [(S)-1,5,10,14-Tetrakis-(toluene-4-sulfonyl)-1,5,10,14-tetraaza-cyclooctadec-6-yl]-methanol

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Technology Process of [(S)-1,5,10,14-Tetrakis-(toluene-4-sulfonyl)-1,5,10,14-tetraaza-cyclooctadec-6-yl]-methanol

There total 6 articles about [(S)-1,5,10,14-Tetrakis-(toluene-4-sulfonyl)-1,5,10,14-tetraaza-cyclooctadec-6-yl]-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 109240-52-0
O¹,O¹²-dimesyl-N⁴,N⁹-ditosyl-4,9-diaza-1,12-dodecanediol

: 109240-50-8
C₁₉H₂₆N₂O₅S₂

: 109240-53-1
[(S)-1,5,10,14-Tetrakis-(toluene-4-sulfonyl)-1,5,10,14-tetraaza-cyclooctadec-6-yl]-methanol

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 80 ℃;
DOI:10.1016/S0040-4039(00)85368-X

Reference yield:

: 15544-47-5
N,N'-ditosyl-1,4-diaminobutane

: 109240-53-1
[(S)-1,5,10,14-Tetrakis-(toluene-4-sulfonyl)-1,5,10,14-tetraaza-cyclooctadec-6-yl]-methanol

Guidance literature:: Multi-step reaction with 3 steps

1: 45 percent / K₂CO₃ / dimethylformamide / 48 h / 95 °C

2: CH₂Cl₂ / 20 °C

3: 55 percent / Cs₂CO₃ / dimethylformamide / 80 °C

With potassium carbonate; caesium carbonate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)85368-X

Reference yield:

: 20803-01-4
N^α,N^δ-Ditosyl-L-ornithin

: 109240-53-1
[(S)-1,5,10,14-Tetrakis-(toluene-4-sulfonyl)-1,5,10,14-tetraaza-cyclooctadec-6-yl]-methanol

Guidance literature:: Multi-step reaction with 2 steps

1: 58 percent / BH₃ / tetrahydrofuran / 24 h / 20 °C

2: 55 percent / Cs₂CO₃ / dimethylformamide / 80 °C

With borane; caesium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)85368-X