N-tert-butoxy-1-[4-(2-cyclopropylethynyl)phenyl]-2-(1,2,4-triazol-1-yl)ethanimine

Base Information

Chemical Name:N-tert-butoxy-1-[4-(2-cyclopropylethynyl)phenyl]-2-(1,2,4-triazol-1-yl)ethanimine
CAS No.:1458958-09-2
Molecular Formula:C₁₉H₂₂N₄O
Molecular Weight:322.41
Hs Code.:

Synonyms:N-tert-butoxy-1-[4-(2-cyclopropylethynyl)phenyl]-2-(1,2,4-triazol-1-yl)ethanimine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-tert-butoxy-1-[4-(2-cyclopropylethynyl)phenyl]-2-(1,2,4-triazol-1-yl)ethanimine

Chemical Property:

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Technology Process of N-tert-butoxy-1-[4-(2-cyclopropylethynyl)phenyl]-2-(1,2,4-triazol-1-yl)ethanimine

There total 3 articles about N-tert-butoxy-1-[4-(2-cyclopropylethynyl)phenyl]-2-(1,2,4-triazol-1-yl)ethanimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1458957-29-3
1-[4-(2-cyclopropylethynyl)phenyl]-2-(1,2,4-triazol-1-yl)ethanone

: 39684-28-1
O-(tert-butyl)hydroxylamine hydrochloride

: 1458958-09-2
N-tert-butoxy-1-[4-(2-cyclopropylethynyl)phenyl]-2-(1,2,4-triazol-1-yl)ethanimine

Guidance literature:: With sodium acetate; In ethanol; Reflux;

Reference yield:

: 99-73-0,132309-76-3
para-bromophenacyl bromide

: 1458958-09-2
N-tert-butoxy-1-[4-(2-cyclopropylethynyl)phenyl]-2-(1,2,4-triazol-1-yl)ethanimine

Guidance literature:: Multi-step reaction with 3 steps

1: N,N-dimethyl-formamide / 1 h / 0 - 5 °C

2: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

3: sodium acetate / ethanol / Reflux

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; sodium acetate; triethylamine; In ethanol; N,N-dimethyl-formamide;

Reference yield:

: 60850-59-1
1-(4-bromophenyl)-2-(1H-1,2,4-triazol-1-yl)-ethanone

: 1458958-09-2
N-tert-butoxy-1-[4-(2-cyclopropylethynyl)phenyl]-2-(1,2,4-triazol-1-yl)ethanimine

Guidance literature:: Multi-step reaction with 2 steps

1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

2: sodium acetate / ethanol / Reflux

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; sodium acetate; triethylamine; In ethanol; N,N-dimethyl-formamide;