Technology Process of C14H17NO3S
There total 5 articles about C14H17NO3S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
bis-triphenylphosphine-palladium(II) chloride; triethylamine;
In
methanol;
at 80 ℃;
for 10h;
Overall yield = 35 %; Overall yield = 20 mg; regioselective reaction;
Schlenk technique;
Inert atmosphere;
DOI:10.1016/j.tetlet.2014.02.087
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate; sodium iodide / 20 - 80 °C
2: potassium tert-butylate / tetrahydrofuran / 0 - 20 °C
3: bis-triphenylphosphine-palladium(II) chloride; triethylamine / methanol / 10 h / 80 °C / Schlenk technique; Inert atmosphere
With
bis-triphenylphosphine-palladium(II) chloride; potassium tert-butylate; potassium carbonate; triethylamine; sodium iodide;
In
tetrahydrofuran; methanol;
DOI:10.1016/j.tetlet.2014.02.087
- Guidance literature:
-
Multi-step reaction with 4 steps
1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 20 °C
2: potassium carbonate; sodium iodide / 20 - 80 °C
3: potassium tert-butylate / tetrahydrofuran / 0 - 20 °C
4: bis-triphenylphosphine-palladium(II) chloride; triethylamine / methanol / 10 h / 80 °C / Schlenk technique; Inert atmosphere
With
bis-triphenylphosphine-palladium(II) chloride; di-isopropyl azodicarboxylate; potassium tert-butylate; potassium carbonate; triethylamine; triphenylphosphine; sodium iodide;
In
tetrahydrofuran; methanol;
1: |Mitsunobu Displacement;
DOI:10.1016/j.tetlet.2014.02.087
