methyl <11(2S)>-11-<2-piperidinyl>>-9-undecenoate

Base Information

Chemical Name:methyl <11(2S)>-11-<2-piperidinyl>>-9-undecenoate
CAS No.:164365-86-0
Molecular Formula:C₂₅H₃₇NO₄
Molecular Weight:415.573
Hs Code.:

methyl <11(2S)>-11-<2-<N-<(benzyloxy)carbonyl>piperidinyl>>-9-undecenoate

Synonyms:methyl <11(2S)>-11-<2-piperidinyl>>-9-undecenoate

Suppliers and Price of methyl <11(2S)>-11-<2-piperidinyl>>-9-undecenoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of methyl <11(2S)>-11-<2-piperidinyl>>-9-undecenoate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of methyl <11(2S)>-11-<2-piperidinyl>>-9-undecenoate

There total 6 articles about methyl <11(2S)>-11-<2-piperidinyl>>-9-undecenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 42843-95-8
<8-(methoxycarbonyl)octyl>triphenylphosphonium iodide

: 143264-54-4
(2S)-N-<(benzyloxy)carbonyl>-2-(formylmethyl)piperidine

: 164365-86-0
methyl <11(2S)>-11-<2-piperidinyl>>-9-undecenoate

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; at 0 ℃;
DOI:10.1039/c39950001015

Reference yield:

: 34418-91-2
2,3,4,5-tetrahydropyridine N-oxide

: 164365-86-0
methyl <11(2S)>-11-<2-piperidinyl>>-9-undecenoate

Guidance literature:: Multi-step reaction with 6 steps

1: 69 percent / toluene / 14 h / Heating

2: 86 percent / tetrabutylammonium fluoride / tetrahydrofuran / 1.5 h / 45 °C

3: 91 percent / H₂, PdCl₂ / methanol / 37 h / 4940 Torr

4: 85 percent / Na₂CO₃ / CH₂Cl₂; H₂O / 14 h / Ambient temperature

5: 84 percent / HIO₄ / tetrahydrofuran; H₂O / 2 h / 0 °C

6: 56 percent / potassium tert-butoxide / tetrahydrofuran / 0.33 h / 0 °C

With potassium tert-butylate; tetrabutyl ammonium fluoride; hydrogen; sodium carbonate; periodic acid; palladium dichloride; In tetrahydrofuran; methanol; dichloromethane; water; toluene;
DOI:10.1021/jo9518258

Reference yield:

: 173425-05-3
<2R,2(1S),3aS>-2-(1-hydroxy-2-methylpropyl)-3,3a,4,5,6,7-hexahydro-2H-isoxazolo<2,3-a>pyridine

: 164365-86-0
methyl <11(2S)>-11-<2-piperidinyl>>-9-undecenoate

Guidance literature:: Multi-step reaction with 4 steps

1: 91 percent / H₂, PdCl₂ / methanol / 37 h / 4940 Torr

2: 85 percent / Na₂CO₃ / CH₂Cl₂; H₂O / 14 h / Ambient temperature

3: 84 percent / HIO₄ / tetrahydrofuran; H₂O / 2 h / 0 °C

4: 56 percent / potassium tert-butoxide / tetrahydrofuran / 0.33 h / 0 °C

With potassium tert-butylate; hydrogen; sodium carbonate; periodic acid; palladium dichloride; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1021/jo9518258