methyl 4-[N-(allyl)-L-phenylalaninylbenzylamino]-1H-pyrrole-2-carboxylate

Base Information

Chemical Name:methyl 4-[N-(allyl)-L-phenylalaninylbenzylamino]-1H-pyrrole-2-carboxylate
CAS No.:1038451-68-1
Molecular Formula:C₂₅H₂₇N₃O₃
Molecular Weight:417.508
Hs Code.:

Synonyms:methyl 4-[N-(allyl)-L-phenylalaninylbenzylamino]-1H-pyrrole-2-carboxylate

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Chemical Property of methyl 4-[N-(allyl)-L-phenylalaninylbenzylamino]-1H-pyrrole-2-carboxylate

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Technology Process of methyl 4-[N-(allyl)-L-phenylalaninylbenzylamino]-1H-pyrrole-2-carboxylate

There total 1 articles about methyl 4-[N-(allyl)-L-phenylalaninylbenzylamino]-1H-pyrrole-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1038451-58-9
methyl 4-(L-phenylalaninylbenzylamino)-1H-pyrrole-2-carboxylate hydrochloride

: 106-95-6
allyl bromide

: 1038451-68-1
methyl 4-[N-(allyl)-L-phenylalaninylbenzylamino]-1H-pyrrole-2-carboxylate

Guidance literature:: methyl 4-(L-phenylalaninylbenzylamino)-1H-pyrrole-2-carboxylate hydrochloride; With sodium hydroxide; In water; ethyl acetate; Inert atmosphere;

With N,O-bis-(trimethylsilyl)-acetamide; In acetonitrile; at 60 ℃; Inert atmosphere;

allyl bromide; In acetonitrile; Inert atmosphere;
DOI:10.1021/ol8009978

Reference yield:

: 1038451-68-1
methyl 4-[N-(allyl)-L-phenylalaninylbenzylamino]-1H-pyrrole-2-carboxylate

: 100-52-7
benzaldehyde

: (3S,5S)-methyl 4-allyl-1,3-dibenzyl-5-phenyl-3H,5H-pyrrolo[3,2-e][1,4]diazepin-2-one-7-carboxylate

: 1038451-97-6
(3S,5R)-methyl 4-allyl-1,3-dibenzyl-5-phenyl-3H,5H-pyrrolo[3,2-e][1,4]diazepin-2-one-7-carboxylate

Guidance literature:: In toluene; for 24h; optical yield given as %de; diastereoselective reaction; Inert atmosphere; Reflux;
DOI:10.1021/ol8009978