9-((trimethylsilyl)ethylnyl)-10-phenyl-9,10-dihydro-9,10-digerma-9,10[1',2']-benzenoanthracene

Base Information

Chemical Name:9-((trimethylsilyl)ethylnyl)-10-phenyl-9,10-dihydro-9,10-digerma-9,10[1',2']-benzenoanthracene
CAS No.:205237-26-9
Molecular Formula:C₂₉H₂₆Ge₂Si
Molecular Weight:547.791
Hs Code.:

Synonyms:9-((trimethylsilyl)ethylnyl)-10-phenyl-9,10-dihydro-9,10-digerma-9,10[1',2']-benzenoanthracene

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Chemical Property of 9-((trimethylsilyl)ethylnyl)-10-phenyl-9,10-dihydro-9,10-digerma-9,10[1',2']-benzenoanthracene

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Technology Process of 9-((trimethylsilyl)ethylnyl)-10-phenyl-9,10-dihydro-9,10-digerma-9,10[1',2']-benzenoanthracene

There total 1 articles about 9-((trimethylsilyl)ethylnyl)-10-phenyl-9,10-dihydro-9,10-digerma-9,10[1',2']-benzenoanthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 205237-23-6
((trimethylsilyl)ethylnyl)germanium trichloride

: 1074-29-9
trichlorophenylgermane

: (o-phenylene)magnesium

: 205237-26-9
9-((trimethylsilyl)ethylnyl)-10-phenyl-9,10-dihydro-9,10-digerma-9,10[1',2']-benzenoanthracene

Guidance literature:: With HCl; In tetrahydrofuran; water; toluene; stirring (-10°C, 1.5 h, 5°C, 2 h), acetylene addn. (-10°C, 5 h), stirring (-10°C, 2 h, 5°C, 1.5 h, room temp., 18 h), HCl (aq) addn.; evapn. (vac.), extg. (toluene), drying (MgSO4), filtering, evapn. (vac.), chromy. (SiO2, n-hexane, C6H6), evapn.; elem. anal.;
DOI:10.1021/om980073f

Reference yield: 93.0%

: 205237-26-9
9-((trimethylsilyl)ethylnyl)-10-phenyl-9,10-dihydro-9,10-digerma-9,10[1',2']-benzenoanthracene

: 7732-18-5
water

: 205237-27-0
9-ethylnyl-10-phenyl-9,10-dihydro-9,10-digerma-9,10[1',2']-benzenoanthracene

Guidance literature:: With KOH; In tetrahydrofuran; water; stirring (1 h); extg. (toluene), drying (MgSO4), filtering, evapn. (vac.); elem. anal.;
DOI:10.1021/om980073f

Reference yield:

: 205237-26-9
9-((trimethylsilyl)ethylnyl)-10-phenyl-9,10-dihydro-9,10-digerma-9,10[1',2']-benzenoanthracene

: 205237-28-1
1,4-bis(9-(10-phenyl-9,10-digermatripticyl))buta-1,3-diyne

Guidance literature:: Multi-step reaction with 2 steps

1: KOH / water; tetrahydrofuran

2: CuCl; O₂ / pyridine

With KOH; CuCl; O₂; In tetrahydrofuran; pyridine; water;
DOI:10.1021/om980073f