N9-(2-O-acetyl-3-deoxy-3-C-dimethylphosphono-5-O-benzoyl-β-D-ribofuranosyl)-adenine

Base Information

Chemical Name:N9-(2-O-acetyl-3-deoxy-3-C-dimethylphosphono-5-O-benzoyl-β-D-ribofuranosyl)-adenine
CAS No.:161821-90-5
Molecular Formula:C₂₁H₂₄N₅O₈P
Molecular Weight:505.424
Hs Code.:

Synonyms:N9-(2-O-acetyl-3-deoxy-3-C-dimethylphosphono-5-O-benzoyl-β-D-ribofuranosyl)-adenine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N9-(2-O-acetyl-3-deoxy-3-C-dimethylphosphono-5-O-benzoyl-β-D-ribofuranosyl)-adenine

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Technology Process of N9-(2-O-acetyl-3-deoxy-3-C-dimethylphosphono-5-O-benzoyl-β-D-ribofuranosyl)-adenine

There total 1 articles about N9-(2-O-acetyl-3-deoxy-3-C-dimethylphosphono-5-O-benzoyl-β-D-ribofuranosyl)-adenine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

: 66224-66-6,66224-67-7,66224-68-8,66224-69-9,134434-48-3,134434-49-4,134454-76-5,134461-75-9
adenine

: 161822-02-2
1,2-di-O-acetyl-3-deoxy-3-C-dimethylphosphono-5-O-benzoyl-α-D-ribofuranose

: 161821-90-5
N9-(2-O-acetyl-3-deoxy-3-C-dimethylphosphono-5-O-benzoyl-β-D-ribofuranosyl)-adenine

Guidance literature:: With tin(IV) chloride; In acetonitrile; for 120h; Ambient temperature;
DOI:10.1016/S0040-4020(01)85564-2

Reference yield: 67.0%

: 161821-90-5
N9-(2-O-acetyl-3-deoxy-3-C-dimethylphosphono-5-O-benzoyl-β-D-ribofuranosyl)-adenine

: 161821-96-1
N9-(3-deoxy-3-C-dimethylphosphono-5-O-benzoyl-β-D-ribofuranosyl)-adenine

Guidance literature:: With hydrazine hydrate; In pyridine; acetic acid; for 24h; Ambient temperature;
DOI:10.1016/S0040-4020(01)85564-2

Reference yield:

: 161821-90-5
N9-(2-O-acetyl-3-deoxy-3-C-dimethylphosphono-5-O-benzoyl-β-D-ribofuranosyl)-adenine

: 161821-97-2
N9-(2,3-dideoxy-3-C-dimethylphosphono-5-O-benzoyl-β-D-ribofuranosyl)-adenine

Guidance literature:: Multi-step reaction with 3 steps

1: 67 percent / H₂NNH₂*H₂O / acetic acid; pyridine / 24 h / Ambient temperature

2: 4-(DMAP) / CH₂Cl₂ / 1 h / Ambient temperature

3: Bu₃SnH, AIBN / toluene / 1 h / 80 °C

With dmap; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; hydrazine hydrate; In pyridine; dichloromethane; acetic acid; toluene;
DOI:10.1016/S0040-4020(01)85564-2