3-Oxocyclohex-1-enyl cinnamate

Base Information

• Chemical Name: 3-Oxocyclohex-1-enyl cinnamate
• CAS No.: 130110-63-3
• Molecular Formula: C₁₅H₁₄O₃
• Molecular Weight: 242.274

Synonyms:3-Oxocyclohex-1-enyl cinnamate

Chemical Property of 3-Oxocyclohex-1-enyl cinnamate

Chemical Property:

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Technology Process of 3-Oxocyclohex-1-enyl cinnamate

There total 1 articles about 3-Oxocyclohex-1-enyl cinnamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

carbon monoxide (201230-82-2) + 1,3-cylohexanedione (504-02-9) + cinnamoyl chloride (102-92-1,17082-09-6) → 3-Oxocyclohex-1-enyl cinnamate (130110-63-3)

Guidance literature:

With triethylamine; In tetrahydrofuran; acetonitrile; at 100 ℃; under 31028.9 Torr;

DOI:10.1016/0040-4039(90)80162-F

Reference yield:

3-Oxocyclohex-1-enyl cinnamate (130110-63-3) → 4-phenyl-3,4,7,8-tetrahydro-2H-chromene-2,5(6H)-dione (27044-91-3)

Guidance literature:

DOI:10.1016/0040-4039(90)80162-F

upstream raw materials:

carbon monoxide

1,3-cylohexanedione

cinnamoyl chloride

Downstream raw materials:

4-phenyl-3,4,7,8-tetrahydro-2H-chromene-2,5(6H)-dione

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