C₅₆H₆₆N₂O₉

Base Information

Chemical Name:C₅₆H₆₆N₂O₉
CAS No.:1601495-62-8
Molecular Formula:C₅₆H₆₆N₂O₉
Molecular Weight:911.148
Hs Code.:

C<sub>56</sub>H<sub>66</sub>N<sub>2</sub>O<sub>9</sub>

Synonyms:C₅₆H₆₆N₂O₉

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Chemical Property of C₅₆H₆₆N₂O₉

Chemical Property:

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Technology Process of C₅₆H₆₆N₂O₉

There total 11 articles about C₅₆H₆₆N₂O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 1601495-60-6
C₅₂H₅₄N₆O₉

: 1601495-62-8
C₅₆H₆₆N₂O₉

Guidance literature:: C₅₂H₅₄N₆O₉; With trimethylphosphane; In dichloromethane; toluene; at 0 - 20 ℃; for 4h; Darkness;

formaldehyd; With sodium cyanoborohydride; In water; acetic acid; acetonitrile; at 0 - 20 ℃; for 2h; pH=4;
DOI:10.1002/anie.201308017

Reference yield:

: 1601496-83-6
C₅₂H₆₀N₆O₈

: 1601495-62-8
C₅₆H₆₆N₂O₉

Guidance literature:: Multi-step reaction with 5 steps

1.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dichloromethane; dimethyl sulfoxide / 3 h / 0 - 20 °C

2.1: potassium carbonate / methanol / 6 h / 0 - 20 °C

3.1: water; bis-[(trifluoroacetoxy)iodo]benzene / acetonitrile / 1 h / 0 °C / Darkness

4.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / [D₃]acetonitrile / 1 h / 0 °C

5.1: trimethylphosphane / dichloromethane; toluene / 4 h / 0 - 20 °C / Darkness

5.2: 2 h / 0 - 20 °C / pH 4

With water; potassium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; bis-[(trifluoroacetoxy)iodo]benzene; trimethylphosphane; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In methanol; dichloromethane; [D₃]acetonitrile; dimethyl sulfoxide; toluene; acetonitrile;
DOI:10.1002/anie.201308017

Reference yield:

: 79383-44-1
methyl 2-methyl-6-methoxybenzoate

: 1601495-62-8
C₅₆H₆₆N₂O₉

Guidance literature:: Multi-step reaction with 11 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C

1.2: 0.33 h / -78 °C

1.3: 21 h / -78 - 20 °C

2.1: boron tribromide / dichloromethane / 6.5 h / -78 - -20 °C

3.1: calcium sulfate; scandium tris(trifluoromethanesulfonate) / 1,2-dichloro-ethane / 2.5 h / -30 - -10 °C / Inert atmosphere

4.1: calcium sulfate; scandium tris(trifluoromethanesulfonate) / 1,2-dichloro-ethane / 20 h / -30 - 28 °C / Inert atmosphere

5.1: tetra-(n-butyl)ammonium iodide; sodium hydride / mineral oil; N,N-dimethyl-formamide / 0.67 h / 0 °C

5.2: 5 h / 0 °C

6.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / -78 - 0 °C

6.2: 2.5 h / -78 °C

7.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dichloromethane; dimethyl sulfoxide / 3 h / 0 - 20 °C

8.1: potassium carbonate / methanol / 6 h / 0 - 20 °C

9.1: water; bis-[(trifluoroacetoxy)iodo]benzene / acetonitrile / 1 h / 0 °C / Darkness

10.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / [D₃]acetonitrile / 1 h / 0 °C

11.1: trimethylphosphane / dichloromethane; toluene / 4 h / 0 - 20 °C / Darkness

11.2: 2 h / 0 - 20 °C / pH 4

With calcium sulfate; lithium aluminium tetrahydride; water; boron tribromide; tetra-(n-butyl)ammonium iodide; sodium hydride; potassium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; bis-[(trifluoroacetoxy)iodo]benzene; scandium tris(trifluoromethanesulfonate); lithium diisopropyl amide; trimethylphosphane; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; methanol; dichloromethane; [D₃]acetonitrile; dimethyl sulfoxide; 1,2-dichloro-ethane; N,N-dimethyl-formamide; toluene; acetonitrile; mineral oil;
DOI:10.1002/anie.201308017