Technology Process of C28H28N6O2
There total 7 articles about C28H28N6O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: hydrazine hydrate / butan-1-ol / 80 °C
2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C
2.2: 0 - 20 °C
3.1: palladium diacetate; tris-(o-tolyl)phosphine; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 36 h / 100 °C / Inert atmosphere
With
palladium diacetate; sodium hydride; hydrazine hydrate; N-ethyl-N,N-diisopropylamine; tris-(o-tolyl)phosphine;
In
N,N-dimethyl-formamide; mineral oil; butan-1-ol;
- Guidance literature:
-
With
palladium diacetate; N-ethyl-N,N-diisopropylamine; tris-(o-tolyl)phosphine;
In
N,N-dimethyl-formamide;
at 100 ℃;
for 36h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: ethanol / 18 h / 20 °C
1.2: 0 - 20 °C
2.1: triethylamine / dichloromethane / 2 h / -78 °C
3.1: palladium diacetate; tris-(o-tolyl)phosphine; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 36 h / 100 °C / Inert atmosphere
With
palladium diacetate; triethylamine; N-ethyl-N,N-diisopropylamine; tris-(o-tolyl)phosphine;
In
ethanol; dichloromethane; N,N-dimethyl-formamide;