methyl (E)-4-{3-[(5-methyl-2-phenyl-1,3-oxazol-4-yl)methoxy]benzyloxyimino}-4-phenylbutyrate

Base Information

Chemical Name:methyl (E)-4-{3-[(5-methyl-2-phenyl-1,3-oxazol-4-yl)methoxy]benzyloxyimino}-4-phenylbutyrate
CAS No.:250601-73-1
Molecular Formula:C₂₉H₂₈N₂O₅
Molecular Weight:484.552
Hs Code.:

Synonyms:methyl (E)-4-{3-[(5-methyl-2-phenyl-1,3-oxazol-4-yl)methoxy]benzyloxyimino}-4-phenylbutyrate

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Chemical Property of methyl (E)-4-{3-[(5-methyl-2-phenyl-1,3-oxazol-4-yl)methoxy]benzyloxyimino}-4-phenylbutyrate

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Technology Process of methyl (E)-4-{3-[(5-methyl-2-phenyl-1,3-oxazol-4-yl)methoxy]benzyloxyimino}-4-phenylbutyrate

There total 5 articles about methyl (E)-4-{3-[(5-methyl-2-phenyl-1,3-oxazol-4-yl)methoxy]benzyloxyimino}-4-phenylbutyrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 25333-24-8
3-benzoylpropionic acid methyl ester

: 250602-87-0
3-[(5-methyl-2-phenyl-1,3-oxazol-4-yl)methoxy]benzyloxyamine

: 250601-73-1
methyl (E)-4-{3-[(5-methyl-2-phenyl-1,3-oxazol-4-yl)methoxy]benzyloxyimino}-4-phenylbutyrate

Guidance literature:: With sodium acetate; acetic acid; In ethanol; for 12h; Heating;
DOI:10.1248/cpb.51.138

Reference yield:

: 159017-85-3
3-[(5-methyl-2-phenyl-1,3-oxazol-4-yl)methoxy]benzaldehyde

: 250601-73-1
methyl (E)-4-{3-[(5-methyl-2-phenyl-1,3-oxazol-4-yl)methoxy]benzyloxyimino}-4-phenylbutyrate

Guidance literature:: Multi-step reaction with 5 steps

1: 84 percent / sodium borohydride / methanol; tetrahydrofuran / 0.5 h / 20 °C

2: 84 percent / thionyl chloride / toluene / 0.5 h / 20 °C

3: 90 percent / K₂CO₃ / dimethylformamide / 20 h / 20 °C

4: 97 percent / hydrazine monohydrate / ethanol; tetrahydrofuran / 3 h / Heating

5: 61 percent / acetic acid; sodium acetate / ethanol / 12 h / Heating

With sodium tetrahydroborate; thionyl chloride; sodium acetate; potassium carbonate; hydrazine hydrate; acetic acid; In tetrahydrofuran; methanol; ethanol; N,N-dimethyl-formamide; toluene;
DOI:10.1248/cpb.51.138

Reference yield:

: 174258-32-3
4-{[3-(chloromethyl)phenoxy]methyl}-5-methyl-2-phenyl-1,3-oxazole

: 250601-73-1
methyl (E)-4-{3-[(5-methyl-2-phenyl-1,3-oxazol-4-yl)methoxy]benzyloxyimino}-4-phenylbutyrate

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / K₂CO₃ / dimethylformamide / 20 h / 20 °C

2: 97 percent / hydrazine monohydrate / ethanol; tetrahydrofuran / 3 h / Heating

3: 61 percent / acetic acid; sodium acetate / ethanol / 12 h / Heating

With sodium acetate; potassium carbonate; hydrazine hydrate; acetic acid; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;
DOI:10.1248/cpb.51.138