(3,5-di-t-butylphenoxy)triphenylbismuth chloride

Base Information

Chemical Name:(3,5-di-t-butylphenoxy)triphenylbismuth chloride
CAS No.:105071-81-6
Molecular Formula:C₃₂H₃₆BiClO
Molecular Weight:681.071
Hs Code.:

Synonyms:(3,5-di-t-butylphenoxy)triphenylbismuth chloride

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Chemical Property of (3,5-di-t-butylphenoxy)triphenylbismuth chloride

Chemical Property:

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Technology Process of (3,5-di-t-butylphenoxy)triphenylbismuth chloride

There total 1 articles about (3,5-di-t-butylphenoxy)triphenylbismuth chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 28719-54-2,507233-69-4,594-30-9
triphenylbismuth dichloride

: 1138-52-9
3,5-Di-tert-butylphenol

: 105071-81-6
(3,5-di-t-butylphenoxy)triphenylbismuth chloride

Guidance literature:: With N,N,N',N'-tetramethylguanidine; In tetrahydrofuran; under Ar, soln. of phenol compd. and guanidine compd. stirred at room temp. for 20 min, soln of Bi-compd. added dropwise over 15 min, stirred for 45 min; evapd., extracted with hexane, evapd. at room temp. to dryness (vac.), crystd. from pentane at -20°C, washed with pentane (-20°C), dried in vac. at room temp., elem. anal.;

Reference yield: 14.0%

: 105071-81-6
(3,5-di-t-butylphenoxy)triphenylbismuth chloride

: 1138-52-9
3,5-Di-tert-butylphenol

: 105071-80-5
3,5-Di-tert-butyl-2-phenylphenol

Guidance literature:: In toluene; for 0.75h; Heating;

Reference yield:

: 105071-81-6
(3,5-di-t-butylphenoxy)triphenylbismuth chloride

: 62787-21-7
3,5-di-tert-butylphenyl phenyl ether

Guidance literature:: Multi-step reaction with 2 steps

1: 14 percent / toluene / 0.75 h / Heating

2: 68 percent / benzene / 4 h / 80 °C

In toluene; benzene;