Technology Process of 6-<4-Methoxy-3-(2-methoxy-1-methylethyl)styryl>-1,5,5-trimethylcyclohexene
There total 6 articles about 6-<4-Methoxy-3-(2-methoxy-1-methylethyl)styryl>-1,5,5-trimethylcyclohexene which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 95 percent / NaH / 1,2-dimethoxy-ethane / 2 h / Ambient temperature
2: 5.00 g / AcOH / 6 h / 35 - 40 °C
3: 10.29 g / benzene / 1 h / Heating
4: 1)BuLi / 1)hexane,benzene, room temp. 15 min., 2) room temp. 1.5 h;
With
n-butyllithium; sodium hydride; acetic acid;
In
1,2-dimethoxyethane; benzene;
DOI:10.1246/bcsj.58.340
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 91.6 percent / diethyl ether
2: 95.7 percent / LiAlH4 / diethyl ether / 1.5 h / Ambient temperature
3: 95 percent / NaH / 1,2-dimethoxy-ethane / 2 h / Ambient temperature
4: 5.00 g / AcOH / 6 h / 35 - 40 °C
5: 10.29 g / benzene / 1 h / Heating
6: 1)BuLi / 1)hexane,benzene, room temp. 15 min., 2) room temp. 1.5 h;
With
lithium aluminium tetrahydride; n-butyllithium; sodium hydride; acetic acid;
In
1,2-dimethoxyethane; diethyl ether; benzene;
DOI:10.1246/bcsj.58.340
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 95.7 percent / LiAlH4 / diethyl ether / 1.5 h / Ambient temperature
2: 95 percent / NaH / 1,2-dimethoxy-ethane / 2 h / Ambient temperature
3: 5.00 g / AcOH / 6 h / 35 - 40 °C
4: 10.29 g / benzene / 1 h / Heating
5: 1)BuLi / 1)hexane,benzene, room temp. 15 min., 2) room temp. 1.5 h;
With
lithium aluminium tetrahydride; n-butyllithium; sodium hydride; acetic acid;
In
1,2-dimethoxyethane; diethyl ether; benzene;
DOI:10.1246/bcsj.58.340
