2-(2-(5-(4-aminophenoxy)carbonyl)amino)-N-[2-(2-acetoxyethoxy)ethyl]-3-amino-1,8-naphthalimide

Base Information

Chemical Name:2-(2-(5-(4-aminophenoxy)carbonyl)amino)-N-[2-(2-acetoxyethoxy)ethyl]-3-amino-1,8-naphthalimide
CAS No.:1422362-73-9
Molecular Formula:C₂₅H₂₃N₃O₇
Molecular Weight:477.474
Hs Code.:

Synonyms:2-(2-(5-(4-aminophenoxy)carbonyl)amino)-N-[2-(2-acetoxyethoxy)ethyl]-3-amino-1,8-naphthalimide

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Chemical Property of 2-(2-(5-(4-aminophenoxy)carbonyl)amino)-N-[2-(2-acetoxyethoxy)ethyl]-3-amino-1,8-naphthalimide

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Technology Process of 2-(2-(5-(4-aminophenoxy)carbonyl)amino)-N-[2-(2-acetoxyethoxy)ethyl]-3-amino-1,8-naphthalimide

There total 4 articles about 2-(2-(5-(4-aminophenoxy)carbonyl)amino)-N-[2-(2-acetoxyethoxy)ethyl]-3-amino-1,8-naphthalimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1422362-72-8
2-(2-(5-(4-nitrophenoxy)carbonyl)amino)-N-[2-(2-acetoxyethoxy)ethyl]-3-amino-1,8-naphthalimide

: 1422362-73-9
2-(2-(5-(4-aminophenoxy)carbonyl)amino)-N-[2-(2-acetoxyethoxy)ethyl]-3-amino-1,8-naphthalimide

Guidance literature:: With palladium on activated charcoal; hydrogen; In ethyl acetate; at 20 ℃;
DOI:10.1039/c3cc38471c

Reference yield:

: 651768-41-1
N-[2-(2-hydroxyethoxy)ethyl]-3-nitro-1,8-naphthalimide

: 1422362-73-9
2-(2-(5-(4-aminophenoxy)carbonyl)amino)-N-[2-(2-acetoxyethoxy)ethyl]-3-amino-1,8-naphthalimide

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / 20 °C

2: palladium on activated charcoal; hydrogen / methanol / 4 h / Reflux

3: acetonitrile / 12 h / 0 °C / Inert atmosphere

4: palladium on activated charcoal; hydrogen / ethyl acetate / 20 °C

With pyridine; palladium on activated charcoal; hydrogen; In methanol; ethyl acetate; acetonitrile;
DOI:10.1039/c3cc38471c

Reference yield:

: 1422362-70-6
N-[2-(2-acetoxyethoxy)ethyl]-3-nitro-1,8-naphthalimide

: 1422362-73-9
2-(2-(5-(4-aminophenoxy)carbonyl)amino)-N-[2-(2-acetoxyethoxy)ethyl]-3-amino-1,8-naphthalimide

Guidance literature:: Multi-step reaction with 3 steps

1: palladium on activated charcoal; hydrogen / methanol / 4 h / Reflux

2: acetonitrile / 12 h / 0 °C / Inert atmosphere

3: palladium on activated charcoal; hydrogen / ethyl acetate / 20 °C

With palladium on activated charcoal; hydrogen; In methanol; ethyl acetate; acetonitrile;
DOI:10.1039/c3cc38471c