2-(2-(5-(4-nitrophenoxy)carbonyl)amino)-N-[2-(2-acetoxyethoxy)ethyl]-3-amino-1,8-naphthalimide

Base Information

Chemical Name:2-(2-(5-(4-nitrophenoxy)carbonyl)amino)-N-[2-(2-acetoxyethoxy)ethyl]-3-amino-1,8-naphthalimide
CAS No.:1422362-72-8
Molecular Formula:C₂₅H₂₁N₃O₉
Molecular Weight:507.456
Hs Code.:

Synonyms:2-(2-(5-(4-nitrophenoxy)carbonyl)amino)-N-[2-(2-acetoxyethoxy)ethyl]-3-amino-1,8-naphthalimide

Suppliers and Price of 2-(2-(5-(4-nitrophenoxy)carbonyl)amino)-N-[2-(2-acetoxyethoxy)ethyl]-3-amino-1,8-naphthalimide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-(2-(5-(4-nitrophenoxy)carbonyl)amino)-N-[2-(2-acetoxyethoxy)ethyl]-3-amino-1,8-naphthalimide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-(2-(5-(4-nitrophenoxy)carbonyl)amino)-N-[2-(2-acetoxyethoxy)ethyl]-3-amino-1,8-naphthalimide

There total 4 articles about 2-(2-(5-(4-nitrophenoxy)carbonyl)amino)-N-[2-(2-acetoxyethoxy)ethyl]-3-amino-1,8-naphthalimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 651768-41-1
N-[2-(2-hydroxyethoxy)ethyl]-3-nitro-1,8-naphthalimide

: 1422362-72-8
2-(2-(5-(4-nitrophenoxy)carbonyl)amino)-N-[2-(2-acetoxyethoxy)ethyl]-3-amino-1,8-naphthalimide

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 20 °C

2: palladium on activated charcoal; hydrogen / methanol / 4 h / Reflux

3: acetonitrile / 12 h / 0 °C / Inert atmosphere

With pyridine; palladium on activated charcoal; hydrogen; In methanol; acetonitrile;
DOI:10.1039/c3cc38471c

Reference yield:

: 1422362-70-6
N-[2-(2-acetoxyethoxy)ethyl]-3-nitro-1,8-naphthalimide

: 1422362-72-8
2-(2-(5-(4-nitrophenoxy)carbonyl)amino)-N-[2-(2-acetoxyethoxy)ethyl]-3-amino-1,8-naphthalimide

Guidance literature:: Multi-step reaction with 2 steps

1: palladium on activated charcoal; hydrogen / methanol / 4 h / Reflux

2: acetonitrile / 12 h / 0 °C / Inert atmosphere

With palladium on activated charcoal; hydrogen; In methanol; acetonitrile;
DOI:10.1039/c3cc38471c

Reference yield:

: 3027-38-1
3-nitro-1,8-naphthalic anhydride

: 1422362-72-8
2-(2-(5-(4-nitrophenoxy)carbonyl)amino)-N-[2-(2-acetoxyethoxy)ethyl]-3-amino-1,8-naphthalimide

Guidance literature:: Multi-step reaction with 4 steps

1: ethanol / 4 h / Reflux

2: pyridine / 20 °C

3: palladium on activated charcoal; hydrogen / methanol / 4 h / Reflux

4: acetonitrile / 12 h / 0 °C / Inert atmosphere

With pyridine; palladium on activated charcoal; hydrogen; In methanol; ethanol; acetonitrile;
DOI:10.1039/c3cc38471c