p-methylphenyl 4,6-O-p-methoxybenzylidene-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:p-methylphenyl 4,6-O-p-methoxybenzylidene-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-1-thio-β-D-glucopyranoside
CAS No.:852570-15-1
Molecular Formula:C₂₄H₂₆Cl₃NO₇S
Molecular Weight:578.898
Hs Code.:

Synonyms:p-methylphenyl 4,6-O-p-methoxybenzylidene-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-1-thio-β-D-glucopyranoside

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Chemical Property of p-methylphenyl 4,6-O-p-methoxybenzylidene-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-1-thio-β-D-glucopyranoside

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Technology Process of p-methylphenyl 4,6-O-p-methoxybenzylidene-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-1-thio-β-D-glucopyranoside

There total 1 articles about p-methylphenyl 4,6-O-p-methoxybenzylidene-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 2186-92-7
p-Anisaldehyde dimethyl acetal

: 220645-20-5
p-methylphenyl 3,4,6-tri-O-acetyl-2-deoxy-1-thio-2-(2,2,2-trichloroethyloxycarbonylamino)-β-D-glucopyranoside

: 852570-15-1
p-methylphenyl 4,6-O-p-methoxybenzylidene-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-1-thio-β-D-glucopyranoside

Guidance literature:: p-methylphenyl 3,4,6-tri-O-acetyl-2-deoxy-1-thio-2-(2,2,2-trichloroethyloxycarbonylamino)-β-D-glucopyranoside; With sodium methylate; In methanol; at 20 ℃; for 6h;

p-Anisaldehyde dimethyl acetal; With camphor-10-sulfonic acid; In acetonitrile; at 20 ℃; for 5h;
DOI:10.1016/j.tet.2005.02.023

Reference yield: 83.0%

: 852570-15-1
p-methylphenyl 4,6-O-p-methoxybenzylidene-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-1-thio-β-D-glucopyranoside

: 98-88-4
benzoyl chloride

: 852570-16-2
p-methylphenyl 3-O-benzoyl-4,6-O-p-methoxybenzylidene-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-1-thio-β-D-glucopyranoside

Guidance literature:: With pyridine; at 0 ℃; for 5h;
DOI:10.1016/j.tet.2005.02.023

Reference yield:

: 852570-15-1
p-methylphenyl 4,6-O-p-methoxybenzylidene-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-1-thio-β-D-glucopyranoside

: 852570-18-4
p-methylphenyl 3-O-benzoyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-1-thio-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / pyridine / 5 h / 0 °C

2: 91 percent / acetic acid / H₂O / 20 °C

With pyridine; acetic acid; In water;
DOI:10.1016/j.tet.2005.02.023