Technology Process of C22H24N2O6
There total 5 articles about C22H24N2O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C23H28N2O7;
With
lithium hydroxide;
In
methanol; water;
at 20 ℃;
for 6h;
With
dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
dichloromethane;
at 20 ℃;
for 1h;
DOI:10.1002/ejoc.201700181
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: lithium hydroxide / water; methanol / 6 h / 20 °C
2.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C
2.2: 3 h / 20 °C
3.1: lithium hydroxide / water; methanol / 6 h / 20 °C
3.2: 1 h / 20 °C
With
oxalyl dichloride; N,N-dimethyl-formamide; lithium hydroxide;
In
methanol; dichloromethane; water;
DOI:10.1002/ejoc.201700181
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydroxide / water / 24 h / Reflux
1.2: 12 h / Reflux
1.3: 95 °C
2.1: lithium hydroxide / water; methanol / 6 h / 20 °C
3.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C
3.2: 3 h / 20 °C
4.1: lithium hydroxide / water; methanol / 6 h / 20 °C
4.2: 1 h / 20 °C
With
oxalyl dichloride; N,N-dimethyl-formamide; sodium hydroxide; lithium hydroxide;
In
methanol; dichloromethane; water;
DOI:10.1002/ejoc.201700181
