4-(benzyloxy)-3-((tert-butyldimethylsilyloxy)methyl)-3-(methoxymethoxy)butan-2-one

Base Information

Chemical Name:4-(benzyloxy)-3-((tert-butyldimethylsilyloxy)methyl)-3-(methoxymethoxy)butan-2-one
CAS No.:1429638-39-0
Molecular Formula:C₂₀H₃₄O₅Si
Molecular Weight:382.572
Hs Code.:

Synonyms:4-(benzyloxy)-3-((tert-butyldimethylsilyloxy)methyl)-3-(methoxymethoxy)butan-2-one

Suppliers and Price of 4-(benzyloxy)-3-((tert-butyldimethylsilyloxy)methyl)-3-(methoxymethoxy)butan-2-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(benzyloxy)-3-((tert-butyldimethylsilyloxy)methyl)-3-(methoxymethoxy)butan-2-one

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Technology Process of 4-(benzyloxy)-3-((tert-butyldimethylsilyloxy)methyl)-3-(methoxymethoxy)butan-2-one

There total 4 articles about 4-(benzyloxy)-3-((tert-butyldimethylsilyloxy)methyl)-3-(methoxymethoxy)butan-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1429638-49-2
5-((benzyloxy)methyl)-8,8,9,9-tetramethyl-5-(prop-1-en-2-yl)-2,4,7-trioxa-8-siladecane

: 1429638-39-0
4-(benzyloxy)-3-((tert-butyldimethylsilyloxy)methyl)-3-(methoxymethoxy)butan-2-one

Guidance literature:: With pyridine; ozone; Sudan-IV; In water; acetone; at 0 ℃; for 0.0833333h; Inert atmosphere;
DOI:10.1021/ol4005799

Reference yield:

: 1429638-47-0
1-(benzyloxy)-2-((tert-butyldimethylsilyloxy)methyl)-3-methylbut-3-en-2-ol

: 1429638-39-0
4-(benzyloxy)-3-((tert-butyldimethylsilyloxy)methyl)-3-(methoxymethoxy)butan-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine; sodium iodide / 1,2-dichloro-ethane / 120 h / 85 °C / Inert atmosphere

2: pyridine; ozone; Sudan-IV / acetone; water / 0.08 h / 0 °C / Inert atmosphere

With pyridine; ozone; N-ethyl-N,N-diisopropylamine; Sudan-IV; sodium iodide; In water; 1,2-dichloro-ethane; acetone;
DOI:10.1021/ol4005799

Reference yield:

: 1429638-46-9
2-(((tert-butyldimethylsilyl)oxy)methyl)-3-methylbut-3-ene-1,2-diol

: 1429638-39-0
4-(benzyloxy)-3-((tert-butyldimethylsilyloxy)methyl)-3-(methoxymethoxy)butan-2-one

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / -40 °C / Inert atmosphere

1.2: -20 °C / 18 Torr / Inert atmosphere

2.1: N-ethyl-N,N-diisopropylamine; sodium iodide / 1,2-dichloro-ethane / 120 h / 85 °C / Inert atmosphere

3.1: pyridine; ozone; Sudan-IV / acetone; water / 0.08 h / 0 °C / Inert atmosphere

With pyridine; sodium hydride; ozone; N-ethyl-N,N-diisopropylamine; Sudan-IV; sodium iodide; In water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetone; mineral oil;
DOI:10.1021/ol4005799