3-O-benzyl-5,6-dideoxy-1,2-O-isopropylidene-6-nitro-5-C-nitromethyl-β-L-arabino-hexofuranose

Base Information

Chemical Name:3-O-benzyl-5,6-dideoxy-1,2-O-isopropylidene-6-nitro-5-C-nitromethyl-β-L-arabino-hexofuranose
CAS No.:78283-51-9
Molecular Formula:C₁₇H₂₂N₂O₈
Molecular Weight:382.37
Hs Code.:

Synonyms:3-O-benzyl-5,6-dideoxy-1,2-O-isopropylidene-6-nitro-5-C-nitromethyl-β-L-arabino-hexofuranose

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Chemical Property of 3-O-benzyl-5,6-dideoxy-1,2-O-isopropylidene-6-nitro-5-C-nitromethyl-β-L-arabino-hexofuranose

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Technology Process of 3-O-benzyl-5,6-dideoxy-1,2-O-isopropylidene-6-nitro-5-C-nitromethyl-β-L-arabino-hexofuranose

There total 3 articles about 3-O-benzyl-5,6-dideoxy-1,2-O-isopropylidene-6-nitro-5-C-nitromethyl-β-L-arabino-hexofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 75-52-5
nitromethane

: 3-O-benzyl-5,6-dideoxy-1,2-O-isopropylidene-6-nitro-β-L-arabino-hex-5-enofuranose

: 78283-51-9
3-O-benzyl-5,6-dideoxy-1,2-O-isopropylidene-6-nitro-5-C-nitromethyl-β-L-arabino-hexofuranose

Guidance literature:: With sodium methylate; In methanol; for 1h; Ambient temperature;
DOI:10.1246/bcsj.54.496

Reference yield:

: 65434-49-3
3-O-benzyl-1,2-O-isopropylidene-α-D-galactofuranose

: 78283-51-9
3-O-benzyl-5,6-dideoxy-1,2-O-isopropylidene-6-nitro-5-C-nitromethyl-β-L-arabino-hexofuranose

Guidance literature:: Multi-step reaction with 3 steps

1: CH₃ONa / methanol / 15 h / Ambient temperature

2: CH₃COONa / acetic anhydride / 48 h / Ambient temperature

3: 66 percent / CH₃ONa / methanol / 1 h / Ambient temperature

With sodium methylate; sodium acetate; In methanol; acetic anhydride;
DOI:10.1246/bcsj.54.496

Reference yield:

: 1-((3aR,5S,6S,6aR)-6-Benzyloxy-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-5-yl)-2-nitro-ethanol

: 78283-51-9
3-O-benzyl-5,6-dideoxy-1,2-O-isopropylidene-6-nitro-5-C-nitromethyl-β-L-arabino-hexofuranose

Guidance literature:: Multi-step reaction with 2 steps

1: CH₃COONa / acetic anhydride / 48 h / Ambient temperature

2: 66 percent / CH₃ONa / methanol / 1 h / Ambient temperature

With sodium methylate; sodium acetate; In methanol; acetic anhydride;
DOI:10.1246/bcsj.54.496