C₄₆H₃₅N₃O₃

Base Information

Chemical Name:C₄₆H₃₅N₃O₃
CAS No.:1211403-60-9
Molecular Formula:C₄₆H₃₅N₃O₃
Molecular Weight:677.802
Hs Code.:

C<sub>46</sub>H<sub>35</sub>N<sub>3</sub>O<sub>3</sub>

Synonyms:C₄₆H₃₅N₃O₃

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Chemical Property of C₄₆H₃₅N₃O₃

Chemical Property:

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Technology Process of C₄₆H₃₅N₃O₃

There total 10 articles about C₄₆H₃₅N₃O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1211403-59-6
C₄₈H₃₉N₃O₃

: 1211403-60-9
C₄₆H₃₅N₃O₃

Guidance literature:: C₄₈H₃₉N₃O₃; With water; sodium hydroxide; In tetrahydrofuran; ethanol; at 50 - 60 ℃; for 4h;

With hydrogenchloride; In tetrahydrofuran; water;

Reference yield:

: 104-94-9
4-methoxy-aniline

: 1211403-60-9
C₄₆H₃₅N₃O₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium t-butanolate / palladium diacetate; tri-tert-butyl phosphine / xylene / 21 h / Inert atmosphere; Reflux

2.1: sodium t-butanolate / palladium diacetate; tri-tert-butyl phosphine / xylene / 19 h / Reflux; Inert atmosphere

3.1: hydrogen bromide; acetic acid / 3 h / Reflux

4.1: sodium hydride / tetrahydrofuran / 0.17 h / 20 °C / Inert atmosphere

4.2: 4 h / 0 °C

5.1: sodium hydride / N,N-dimethyl-formamide / 15.5 h / 20 - 65 °C / Inert atmosphere

6.1: sodium hydroxide; water / ethanol; tetrahydrofuran / 4 h / 50 - 60 °C

With water; hydrogen bromide; sodium hydride; acetic acid; sodium hydroxide; sodium t-butanolate; tri-tert-butyl phosphine; palladium diacetate; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide; xylene;

Reference yield:

: 90-14-2
1-Iodonaphthalene

: 1211403-60-9
C₄₆H₃₅N₃O₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium t-butanolate / palladium diacetate; tri-tert-butyl phosphine / xylene / 21 h / Inert atmosphere; Reflux

2.1: sodium t-butanolate / palladium diacetate; tri-tert-butyl phosphine / xylene / 19 h / Reflux; Inert atmosphere

3.1: hydrogen bromide; acetic acid / 3 h / Reflux

4.1: sodium hydride / tetrahydrofuran / 0.17 h / 20 °C / Inert atmosphere

4.2: 4 h / 0 °C

5.1: sodium hydride / N,N-dimethyl-formamide / 15.5 h / 20 - 65 °C / Inert atmosphere

6.1: sodium hydroxide; water / ethanol; tetrahydrofuran / 4 h / 50 - 60 °C

With water; hydrogen bromide; sodium hydride; acetic acid; sodium hydroxide; sodium t-butanolate; tri-tert-butyl phosphine; palladium diacetate; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide; xylene;