[PdCl(CH₃(CH₂)7OC₆H₃CHNC₆H₄O(CH₂)7CH₃)]2

Base Information

Chemical Name:[PdCl(CH₃(CH₂)7OC₆H₃CHNC₆H₄O(CH₂)7CH₃)]2
CAS No.:154295-41-7
Molecular Formula:C₅₈H₈₄Cl₂N₂O₄Pd₂
Molecular Weight:1157.06
Hs Code.:

[PdCl(CH<sub>3</sub>(CH<sub>2</sub>)7OC<sub>6</sub>H<sub>3</sub>CHNC<sub>6</sub>H<sub>4</sub>O(CH<sub>2</sub>)7CH<sub>3</sub>)]2

Synonyms:[PdCl(CH₃(CH₂)7OC₆H₃CHNC₆H₄O(CH₂)7CH₃)]2

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Chemical Property of [PdCl(CH₃(CH₂)7OC₆H₃CHNC₆H₄O(CH₂)7CH₃)]2

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Technology Process of [PdCl(CH₃(CH₂)7OC₆H₃CHNC₆H₄O(CH₂)7CH₃)]2

There total 1 articles about [PdCl(CH₃(CH₂)7OC₆H₃CHNC₆H₄O(CH₂)7CH₃)]2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 7647-01-0,15364-23-5
hydrogenchloride

: 2Pd⁽²⁺⁾*2CH₃COO^(1-)*2CH₃(CH₂)7OC₆H₃CHNC₆H₄O(CH₂)7CH₃^(1-)=[Pd(CH₃COO)(CH₃(CH₂)7OC₆H₃CHNC₆H₄O(CH₂)7CH₃)]2

: 154295-41-7
[PdCl(CH₃(CH₂)7OC₆H₃CHNC₆H₄O(CH₂)7CH₃)]2

Guidance literature:: In methanol; dichloromethane; slow addn. of equimolar amt. of HCl (in MeOH) to Pd-complex soln. (in CH2Cl2), stirring for 1 h; evapn., chromy. (SiO2, CH2Cl2), addn. of Me2CO, crystn. on concn., filtration, washing (Me2CO), drying in air; elem. anal.;
DOI:10.1016/0022-328X(95)05771-G

Reference yield: 94.0%

: 154295-41-7
[PdCl(CH₃(CH₂)7OC₆H₃CHNC₆H₄O(CH₂)7CH₃)]2

: potassium (R)-2-chloropropionate

: [Pd((R)-2-chloropropionate)(CH₃(CH₂)7OC₆H₃CHNCC₆H₄O(CH₂)7CH₃)]2

Guidance literature:: In dichloromethane; acetone; stirring Pd-complex with 1.1 equiv. of carboxylate (in Me2CO/CH2Cl2=1:1,12 h); evapn., extn. into CH2Cl2, filtration, addn. of EtOH, concn., crystn., filtration, washing (EtOH), drying in air; elem. anal.;
DOI:10.1016/0022-328X(95)05771-G

Reference yield: 85.0%

: 1118-66-7
4-amino-3-penten-2-one

: 154295-41-7
[PdCl(CH₃(CH₂)7OC₆H₃CHNC₆H₄O(CH₂)7CH₃)]2

: 173449-17-7
Pd(CH₃(CH₂)7OC₆H₃CHNC₆H₄O(CH₂)7CH₃)(4-amino-3-penten-2-onate)

Guidance literature:: With potassium carbonate; In dichloromethane; byproducts: K(CH3NHCHCOCH3), KCl; addn. of 1.1 equiv. of aminopentenone and excess K2CO3 to Pd-complex soln., stirring overnight; evapn., extn. into CH2Cl2, filtration off of KCl and K(CH3NHCHCOCH3), addn. of EtOH, crystn. on concn., filtration, washing (EtOH), drying in air; elem. anal.;
DOI:10.1016/0022-328X(95)05771-G