methyl 2,4-dimethoxy-6-<1-(p-tolylsulfonyl)-7-methoxycarbonyl heptyl> benzoate

Base Information

Chemical Name:methyl 2,4-dimethoxy-6-<1-(p-tolylsulfonyl)-7-methoxycarbonyl heptyl> benzoate
CAS No.:130877-75-7
Molecular Formula:C₂₆H₃₄O₈S
Molecular Weight:506.617
Hs Code.:

Synonyms:methyl 2,4-dimethoxy-6-<1-(p-tolylsulfonyl)-7-methoxycarbonyl heptyl> benzoate

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Chemical Property of methyl 2,4-dimethoxy-6-<1-(p-tolylsulfonyl)-7-methoxycarbonyl heptyl> benzoate

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Technology Process of methyl 2,4-dimethoxy-6-<1-(p-tolylsulfonyl)-7-methoxycarbonyl heptyl> benzoate

There total 9 articles about methyl 2,4-dimethoxy-6-<1-(p-tolylsulfonyl)-7-methoxycarbonyl heptyl> benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 539-87-7
oxocan-2-one

: 130877-75-7
methyl 2,4-dimethoxy-6-<1-(p-tolylsulfonyl)-7-methoxycarbonyl heptyl> benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: conc. H₂SO₄ / 2 h / Ambient temperature

2: 80 percent / Et₃N / CH₂Cl₂ / 2 h / Ambient temperature

3: NaI, NaHCO₃ / acetone / 72 h / Ambient temperature

4: 1.) LDA, 2.) HMPA / 1.) THF, -78 deg C, 1 h, 2.) 5 min

With N,N,N,N,N,N-hexamethylphosphoric triamide; sulfuric acid; sodium hydrogencarbonate; triethylamine; sodium iodide; lithium diisopropyl amide; In dichloromethane; acetone;
DOI:10.1016/0957-4166(90)90013-Z

Reference yield:

: 6110-37-8
methyl 2,4-dimethoxy-6-methylbenzoate

: 130877-75-7
methyl 2,4-dimethoxy-6-<1-(p-tolylsulfonyl)-7-methoxycarbonyl heptyl> benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) LDA / 1.) THF, -78 deg C, 15 min, 2.) 5 min

2: 94 percent / m-chloroperbenzoic acid (m-CPBA) / CH₂Cl₂ / 1 h / Ambient temperature

3: 1.) LDA, 2.) HMPA / 1.) THF, -78 deg C, 1 h, 2.) 5 min

With N,N,N,N,N,N-hexamethylphosphoric triamide; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; In dichloromethane;
DOI:10.1016/0957-4166(90)90013-Z

Reference yield:

: 14565-11-8
methyl 7-hydroxyheptanoate

: 130877-75-7
methyl 2,4-dimethoxy-6-<1-(p-tolylsulfonyl)-7-methoxycarbonyl heptyl> benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / Et₃N / CH₂Cl₂ / 2 h / Ambient temperature

2: NaI, NaHCO₃ / acetone / 72 h / Ambient temperature

3: 1.) LDA, 2.) HMPA / 1.) THF, -78 deg C, 1 h, 2.) 5 min

With N,N,N,N,N,N-hexamethylphosphoric triamide; sodium hydrogencarbonate; triethylamine; sodium iodide; lithium diisopropyl amide; In dichloromethane; acetone;
DOI:10.1016/0957-4166(90)90013-Z