1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2-bromoimidazole-4,5-dicarboxylic acid dibutyl ester

Base Information

Chemical Name:1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2-bromoimidazole-4,5-dicarboxylic acid dibutyl ester
CAS No.:945229-50-5
Molecular Formula:C₃₉H₃₉BrN₂O₁₁
Molecular Weight:791.649
Hs Code.:

Synonyms:1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2-bromoimidazole-4,5-dicarboxylic acid dibutyl ester

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Chemical Property of 1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2-bromoimidazole-4,5-dicarboxylic acid dibutyl ester

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Technology Process of 1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2-bromoimidazole-4,5-dicarboxylic acid dibutyl ester

There total 1 articles about 1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2-bromoimidazole-4,5-dicarboxylic acid dibutyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 6974-32-9
1-O-acetyl-2,3,5-tri-O-benzoyl-β-D-ribofuranose

: 872182-61-1
dibutyl 2-bromo-1H-imidazole-4,5-dicarboxylate

: 945229-50-5
1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2-bromoimidazole-4,5-dicarboxylic acid dibutyl ester

Guidance literature:: With chloro-trimethyl-silane; trifluorormethanesulfonic acid; 1,1,1,3,3,3-hexamethyl-disilazane; In acetonitrile; for 1.5h;
DOI:10.1016/j.bmc.2007.04.043

Reference yield: 74.8%

: 945229-50-5
1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2-bromoimidazole-4,5-dicarboxylic acid dibutyl ester

: 5720-07-0
4-methoxyphenylboronic acid

: 1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2-p-methoxyphenylimidazole-4,5-dicarboxylic acid dibutyl ester

Guidance literature:: With sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; water; benzene; for 60h; Heating;
DOI:10.1016/j.bmc.2007.04.043

Reference yield: 53.5%

: 945229-50-5
1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2-bromoimidazole-4,5-dicarboxylic acid dibutyl ester

: 98-80-6
phenylboronic acid

: 1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2-phenylimidazole-4,5-dicarboxylic acid dibutyl ester

Guidance literature:: With sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; water; benzene; Heating;
DOI:10.1016/j.bmc.2007.04.043